Corrosion inhibitor for offshore oilfield water treatment system and preparation method thereof
A water treatment system and offshore oilfield technology, applied in earthwork drilling and production, wellbore/well components, etc., can solve the problems of low corrosion inhibition efficiency, large amount of formula used, and large side effects, and achieve high corrosion inhibition rate, simple formula, Effect with few side effects
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[0023] The preparation method of corrosion inhibitor for offshore oilfield water treatment system of the present invention comprises the following steps: dissolving sodium phosphate and naphthenic acid imidazoline completely with hot water respectively, putting the above-mentioned aqueous solution into a reaction kettle, and heating up to 90- 100°C, make sodium phosphate and naphthenic acid imidazoline undergo condensation reaction, the reaction time is 3 hours; after the reaction product is refluxed to separate the water, continue to add glutaraldehyde, 2-hydroxyphosphonoacetic acid and methyl acrylate, and heat up under stirring To 120-140 ℃, make the raw materials undergo polymerization reaction, the reaction time is 2 hours, and obtain a uniform viscous liquid; fully condense to room temperature, and use ethylene glycol as a solvent to dilute.
[0024] A water separator is set in the reaction kettle, and the reaction product is separated by the water separator after the con...
Embodiment 1
[0027] Corrosion inhibitor for offshore oilfield water treatment system of the present invention, each raw material is respectively: sodium phosphate 50g, naphthenic acid imidazoline 100g, glutaraldehyde 30g, 2-hydroxyphosphonoacetic acid 60g, methyl acrylate 1.5g, reaction finishes Then dilute with ethylene glycol as solvent.
[0028] The mass of methyl acrylate is 5% of the mass of glutaraldehyde, and the methyl acrylate is used as an initiator of the polymerization reaction.
[0029] During preparation, sodium phosphate and naphthenic acid imidazoline were completely dissolved in hot water respectively, and the above aqueous solution was put into a reaction kettle, and the temperature was raised to 90°C to cause condensation reaction between sodium phosphate and naphthenic acid imidazoline, and the reaction time was 3 hours; after the reaction product was refluxed to separate the water, continue to add glutaraldehyde, 2-hydroxyphosphonoacetic acid and methyl acrylate, and r...
Embodiment 2
[0037] Corrosion inhibitor for offshore oilfield water treatment system of the present invention, each raw material is respectively: sodium phosphate 70g, naphthenic acid imidazoline 120g, glutaraldehyde 50g, 2-hydroxyphosphonoacetic acid 50g, methyl acrylate 2.5g, reaction finishes Then dilute with ethylene glycol as solvent.
[0038] The mass of methyl acrylate is 5% of the mass of glutaraldehyde, and the methyl acrylate is used as an initiator of the polymerization reaction.
[0039] During preparation, sodium phosphate and naphthenic acid imidazoline were completely dissolved in hot water respectively, and the above aqueous solution was put into the reaction kettle, and the temperature was raised to 100°C to cause condensation reaction of sodium phosphate and naphthenic acid imidazoline. The reaction time was 3 Hours; after the reaction product was refluxed to separate the water, continue to add glutaraldehyde, 2-hydroxyphosphonoacetic acid and methyl acrylate, and heat up...
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Abstract
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