Solvent for capturing CO2 and preparation method of solvent for capturing CO2
A technology of solvent and catalyst, which is applied in the field of CO2 capture solvent and its preparation, can solve the problems of high desorption energy consumption, easy volatilization, large DMC circulation volume, etc., achieves wide application prospects, large absorption capacity, and simple and easy synthesis method line effect
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[0015] The present invention will be further described below in conjunction with the embodiments, but the protection scope of the present invention is not limited thereto. Example 1
[0016] Take 108g of dimethyl carbonate and 94g of diethyl carbonate, then add 43g of ethylene glycol, 27g of butanediol, and then add 0.2g of titanium dioxide (TiO 2 ), the reaction was stirred at 120kPa and 110°C for 3h, and the methanol was removed to obtain CO 2 Solvent.
[0017] The solvent obtained was measured, and the measured molecular weight was 266, the viscosity was 5.33 mPa.s, and the density was 1.12 g / cm3. Use this solvent to absorb CO at 25°C and 0.5MPa 2 , CO 2 The solubility in it is 55.6gCO 2 / g solvent.
Example Embodiment
[0018] Example 2
[0019] Take 86g ethyl methyl carbonate and 122g propylene carbonate, then add 40g ethylene glycol, 32g butanediol, and then add 0.1g aluminum oxide (Al 2 O 3 ) And 0.2g zinc oxide (ZnO), stirred and reacted at 110kPa, 130℃ for 3h, stripped off methanol, obtained for CO absorption 2 Solvent.
[0020] Measure the obtained solvent, the measured molecular weight is 289, viscosity is 6.24mPa.s, density is 1.18g / cm 3 . Use this solvent to absorb CO at 25°C and 0.5MPa 2 , CO 2 The solubility in it is 64.3gCO 2 / g solvent.
Example Embodiment
[0021] Example 3
[0022] Take 58g of dimethyl succinate and 144g of dimethyl carbonate, then add 45g of ethylene glycol, 35g of butanediol, and then add 0.1g of tetrabutylammonium bromide (C 16 H 36 BrN) and 0.1g cetyltrimethylammonium bromide quaternary ammonium salt (C 19 H 42 BrN), stirred and reacted at 125kPa, 155°C for 3h, and removed methanol to obtain CO absorption 2 Solvent.
[0023] Measure the obtained solvent, the measured molecular weight is 308, viscosity is 6.24mPa.s, density is 1.18g / cm 3 . Use this solvent to absorb CO at 25°C and 0.5MPa 2 , CO 2 The solubility in it is 71.3gCO 2 / g solvent.
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