Liquid crystal display element and sealing compound for liquid crystal display elements
A technology for liquid crystal display elements and sealants, which can be used in instruments, nonlinear optics, optics, etc., can solve the problems of liquid crystal leakage, contamination of liquid crystal, and seal damage, and achieve the effects of liquid crystal pollution suppression, seal damage suppression, and excellent display performance.
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Embodiment 1
[0085] (Manufacture of sealant 1 for liquid crystal display elements)
[0086] 70 parts by weight of bisphenol A type epoxy acrylate (manufactured by Daicel-Allnex, "EBECRYL3700") and 30 parts by weight of bisphenol F type epoxy resin (manufactured by Mitsubishi Chemical Corporation, "jER806") were blended as a curable resin. 7 parts by weight of a polymeric azo initiator (manufactured by Wako Pure Chemical Industries, Ltd., "VPE-0201") as a thermal radical polymerization initiator, sebacic acid dihydrazide (manufactured by Otsuka Chemical Co., Ltd., " SDH") 8 parts by weight, 25 parts by weight of soft particles A as soft particles, silicon dioxide (manufactured by Admatechs, "Admafine SO-C2", average particle size 0.5 μm) as a filler, 10 parts by weight and silane 1 part by weight of 3-glycidoxypropyltrimethoxysilane (manufactured by Shin-Etsu Chemical Industry Co., Ltd., "KBM-403") as a coupling agent, using a planetary agitator (manufactured by Thinky Company, "degassing R...
Embodiment 2
[0090] (Manufacture of sealant 2 for liquid crystal display elements)
[0091] 70 parts by weight of bisphenol A type epoxy acrylate (manufactured by Daicel-Allnex, "EBECRYL3700") and 30 parts by weight of bisphenol F type epoxy resin (manufactured by Mitsubishi Chemical Corporation, "jER806") were blended as a curable resin. 7 parts by weight of a polymeric azo initiator (manufactured by Wako Pure Chemical Industries, Ltd., "VPE-0201") as a thermal radical polymerization initiator, sebacic acid dihydrazide (manufactured by Otsuka Chemical Co., Ltd., " SDH") 8 parts by weight, 20 parts by weight of soft particles A and 5 parts by weight of soft particles B, silicon dioxide (manufactured by Admatechs, "Admafine SO-C2", average particle diameter 0.5 μm) and 1 part by weight of 3-glycidoxypropyltrimethoxysilane (manufactured by Shin-Etsu Chemical Co., Ltd., "KBM-403") as a silane coupling agent, using a planetary agitator (Thinky Corporation "Degassing Rentaro"), and then unifor...
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