A preparation method of modified nano-catalyst zinc oxide antibacterial ceramics
A technology of nano-catalyst and antibacterial ceramics is applied in the field of preparation of modified nano-catalyst zinc oxide antibacterial ceramics, which can solve the problems such as difficult integration of inorganic antibacterial agent and ceramic base glaze, color distortion on the surface of antibacterial ceramics, poor durability, etc. Fast disinfection effect, good durability and good stability
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Embodiment 1
[0030] A method for preparing modified nano-catalyst zinc oxide antibacterial ceramics includes the following manufacturing steps:
[0031] (1) Preparation of modified catalyst zinc oxide powder: first modify the catalyst zinc oxide, the modification method is to place the catalyst zinc oxide powder in isopropanol containing 2% polyoxyethylene sorbitan fatty acid ester To achieve a single particle dispersion state through sand milling treatment, add tetraethoxysilane to the dispersion to keep the system temperature higher than 60°C without boiling, add water dropwise, stir and age for 5 min, cool to room temperature, filter, Rinse with deionized water until the conductivity of the filtrate is less than 8μS / cm. After the filter cake is obtained, it is rinsed with isopropanol, dried, crushed and calcined to obtain a modified catalyst zinc oxide powder with an inorganic surface treatment;
[0032] (2) Preparation of modified nano-catalyst zinc oxide: The modified catalyst zinc oxide p...
Embodiment 2
[0040] A method for preparing modified nano-catalyst zinc oxide antibacterial ceramics includes the following manufacturing steps:
[0041] (1) Preparation of modified catalyst zinc oxide powder: first modify the catalyst zinc oxide, the modification method is to place the catalyst zinc oxide powder in isopropanol containing 2% polyoxyethylene sorbitan fatty acid ester To achieve a single particle dispersion state through sand milling treatment, add tetraethoxysilane to the dispersion to keep the system temperature higher than 60°C without boiling, add water dropwise, stir and age for 12 minutes, cool to room temperature, filter, Rinse with deionized water until the conductivity of the filtrate is less than 8μS / cm. After the filter cake is obtained, it is rinsed with isopropanol, dried, crushed and calcined to obtain a modified catalyst zinc oxide powder with an inorganic surface treatment;
[0042] (2) Preparation of modified nano-catalyst zinc oxide: the modified catalyst zinc ox...
Embodiment 3
[0050] A method for preparing modified nano-catalyst zinc oxide antibacterial ceramics includes the following manufacturing steps:
[0051] (1) Preparation of modified catalyst zinc oxide powder: first modify the catalyst zinc oxide, the modification method is to place the catalyst zinc oxide powder in isopropanol containing 2% polyoxyethylene sorbitan fatty acid ester To achieve a single particle dispersion state through sand milling treatment, add tetraethoxysilane to the dispersion to keep the system temperature higher than 60°C without boiling, add water dropwise, stir and age for 20 min, cool to room temperature, filter, Rinse with deionized water until the conductivity of the filtrate is less than 8μS / cm. After the filter cake is obtained, it is rinsed with isopropanol, dried, crushed and calcined to obtain a modified catalyst zinc oxide powder with an inorganic surface treatment;
[0052] (2) Preparation of modified nano-catalyst zinc oxide: the modified catalyst zinc oxide ...
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