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A kind of environment-friendly smelting silicon ore catalyst and preparation method thereof

A silicon ore and catalyst technology, used in chemical instruments and methods, catalyst activation/preparation, physical/chemical process catalysts, etc., can solve the problems of waste of resources, large environmental pollution, and the catalyst cannot fully contact the silicon ore, etc., to improve plasticity. , the effect of increasing the specific surface area and improving the fineness

Active Publication Date: 2018-12-07
TANGSHAN ZHENGFENG IRON & STEEL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In the process of extracting silicon from silicon ore, catalysts are often used as a means to accelerate the reaction and improve the purity of silicon. However, due to the large solid-solid phase particles, the catalyst cannot fully contact the silicon ore, resulting in waste of resources. The main components of ore catalysts are copper and zinc, which are extremely polluting to the environment. Therefore, it is necessary to develop a catalyst that can fully contact silicon ore to maximize its effectiveness.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] The preparation method of a kind of environment-friendly smelting silicon ore catalyst that the present invention proposes comprises the following steps:

[0020] S1. Preheating: After vacuuming the first processing equipment, nitrogen gas is introduced, and then the temperature of the first processing equipment is raised to 660°C;

[0021] S2. Mixing and sintering: mix 52 parts of copper powder, 45 parts of zinc powder and 3 parts of aluminum powder in parts by weight, put them into the first processing equipment after preheating, and raise the first processing equipment and its The temperature of the content reaches 1200°C, and then heats it for 35 minutes to obtain material A; among them, the bulk density of copper powder is 2.88g / cm 3 , the bulk density of zinc powder is 2.4g / cm 3 , the bulk density of aluminum powder is 1.2 g / cm 3 ;The particle size of copper powder is 0.084mm, the particle size of zinc powder is 0.005mm, and the particle size of aluminum powder...

Embodiment 2

[0025] The preparation method of a kind of environment-friendly smelting silicon ore catalyst that the present invention proposes comprises the following steps:

[0026] S1. Preheating: After vacuuming the first processing equipment, nitrogen gas is introduced, and then the temperature of the first processing equipment is raised to 620°C;

[0027] S2. Mixing and sintering: Mix 55 parts of copper powder, 40 parts of zinc powder and 5 parts of aluminum powder in parts by weight, put them into the first processing equipment after preheating, and raise the first processing equipment and its The temperature of the content reaches 1400°C, and then keeps warm for 30 minutes to obtain material A; among them, the bulk density of copper powder is 2.96g / cm 3 , the bulk density of zinc powder is 1.8g / cm 3 , the bulk density of aluminum powder is 1.5 g / cm 3; The particle size of copper powder is 0.072mm, the particle size of zinc powder is 0.01mm, and the particle size of aluminum powde...

Embodiment 3

[0031] The preparation method of a kind of environment-friendly smelting silicon ore catalyst that the present invention proposes comprises the following steps:

[0032] S1. Preheating: After vacuuming the first processing equipment, nitrogen gas is introduced, and then the temperature of the first processing equipment is raised to 650°C;

[0033] S2. Mixing and sintering: Mix 56 parts of copper powder, 48 parts of zinc powder and 3.5 parts of aluminum powder in parts by weight, put them into the first processing equipment after preheating, and raise the first processing equipment and its The temperature of the content reaches 1300°C, and then keeps warm for 33 minutes to obtain material A; among them, the bulk density of copper powder is 2.92g / cm 3 , the bulk density of zinc powder is 2.2g / cm 3 , the bulk density of aluminum powder is 1.3 g / cm 3; The particle size of copper powder is 0.082mm, the particle size of zinc powder is 0.006mm, and the particle size of aluminum po...

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Abstract

The invention discloses a preparing method of environment-friendly smelting wollastonite accelerant. The preparing method includes the following steps that first processing equipment is vacuumized, nitrogen is introduced, and then the first processing equipment is preheated; copper powder, zinc powder and aluminum powder are mixed uniformly and put into the preheated first processing equipment, and the temperature of the first processing equipment and the content is raised to obtain a material A; then the material A is cooled and formed in a stretched mode to obtain a material B; the material B is used as the positive and negative poles of arc power consumption self-degrading, the positive and negative poles are put into second processing equipment at the same time, and then supersonic speed arc jet gas atomization is carried out on the material B to obtain the environment-friendly smelting wollastonite accelerant. The invention further discloses environment-friendly smelting wollastonite accelerant. The prepared smelting wollastonite accelerant is high in purity, high in fineness, capable of making full contact with wollastonite and suitable for a wollastonite smelting enterprise.

Description

technical field [0001] The invention relates to the technical field of catalyst preparation, in particular to an environment-friendly catalyst for smelting silicon ore and a preparation method thereof. Background technique [0002] In the process of extracting silicon from silicon ore, catalysts are often used as a means to accelerate the reaction and improve the purity of silicon. However, due to the large solid-solid phase particles, the catalyst cannot fully contact the silicon ore, resulting in waste of resources. The main components of ore catalysts are copper and zinc, which are extremely polluting to the environment. Therefore, it is necessary to develop a catalyst that can fully contact with silicon ore to maximize its effectiveness. Contents of the invention [0003] Based on the technical problems in the background technology, the present invention proposes an environmentally friendly catalyst for smelting silicon ore and its preparation method, which has high pu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J23/80B01J37/34B01J35/10B01J35/08C22C9/04C22C1/02B22F9/14
CPCB01J23/80B01J35/08B01J35/1004B01J37/342B22F9/14C22C1/02C22C9/04
Inventor 李芹
Owner TANGSHAN ZHENGFENG IRON & STEEL CO LTD
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