A sterile medical ultrasonic coupling patch and preparation method thereof
An ultrasonic coupling and patch technology, which is applied in the field of coupling patches, can solve the problems of easy degradation and loss of viscosity, etc., and achieve the effects of improving salt resistance, non-sensitization, and excellent biocompatibility
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Embodiment 1
[0037] Example 1 Preparation and performance testing of modified Tianqing glue
[0038] The raw materials for the preparation of modified Tianqing glue in groups A-D are shown in the following table:
[0039] Group
Group A
Group B
Group C
Group D
Tianqing rubber powder: vinylpyrrolidone (mass ratio)
1:3
1:4
1:5
1:6
[0040] Preparation:
[0041] (1) Take a certain amount of Tianqing rubber powder and disperse it in cold water to prepare a glue with a mass fraction of 0.4%. Under stirring, add 1mol / L hydrochloric acid solution to adjust the pH to 6, and then slowly add it to the glue. Slowly add vinyl pyrrolidone dropwise, continue to stir for 20 minutes, then ultrasonically shake the glue for 10 minutes, and pour nitrogen into it to obtain a mixture for use;
[0042] (2) Subject the mixture obtained in step (1) to γ-ray radiation treatment for 12 minutes, with a radiation dose of 3-20 kGy, and then take it out and leave it for 3 hours. Under stirring, add 2 times the volu...
Embodiment 2-6 and comparative example 1-3
[0051] Preparation of Example 2-6 and Comparative Example 1-3 Sterile Medical Ultrasound Coupling Patch
[0052] The sterile medical ultrasonic coupling patch of Examples 2-6 and Comparative Examples 1-3 of the present invention is composed of the components in percentage by weight as described in the following table:
[0053]
Embodiment 2
[0054] The preparation method of Example 2 is:
[0055] (1) Add water to the acrylate-based polyurethane, stir until it is completely dissolved, and then add modified Tianqing glue in small amounts in several times, shake and dissolve for 40 minutes to obtain a mixture;
[0056] (2) Add propylene glycol alginate and propylene glycol monooleate to the mixture obtained in step (1), raise the temperature to 50°C, keep it warm and continue stirring for 25 minutes, then add polyethylene glycol and sodium pyrrolidone carboxylate, stir and mix evenly;
[0057] (3) After the material obtained in step (2) is cooled to room temperature, the diimidazolidinyl urea is added, and the mixture is evenly stirred to prepare a finished liquid;
[0058] (4) Vacuum the finished liquid to defoam for 8 minutes, then inject it into the mold under vacuum conditions, cure, demold and perform ultraviolet sterilization, and then package to obtain a sterile medical ultrasonic coupling patch. The described ultravio...
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