A kind of anti-fresh cement efflorescence primer styrene-acrylic emulsion and preparation method thereof
A styrene-acrylic emulsion and cement technology, applied in the direction of coating, can solve the problems of difficult to ensure the uniformity of the acid treatment layer, increase the construction cost, neutralization of the acid layer, etc., to improve the compactness and stability, and the reaction speed is fast. , the effect of improving the penetration ability
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[0036] The preparation method of anti-fresh cement efflorescence primer styrene-acrylic emulsion of the present invention comprises the following steps:
[0037] (1) Pre-emulsification
[0038] a: Under normal temperature and pressure, mix 1-2 parts of anionic emulsifier and 20-30 parts of water in a pre-emulsification tank, stir well until dissolved;
[0039] b: Add styrene, methyl methacrylate, isooctyl acrylate, butyl acrylate, acrylic acid, methacrylic acid, methacrylamide and cross-linking monomer to the mixture obtained in step a, and keep stirring until uniform The pre-emulsion can be obtained;
[0040] (2) Polymerization
[0041] c: Add 60-100 parts of water and 4-18 parts of anionic emulsifier to the bottom of the reaction kettle, heat up to 80-90°C while stirring, then add special functional monomers, and stir for 20-40 minutes;
[0042] d: Add the pre-emulsion obtained in step b and 0.1-0.8 parts of initiator dropwise to the mixture obtained in step c to react, the...
Embodiment 1
[0050] The anti-fresh cement efflorescence primer styrene-acrylic emulsion of the present invention comprises water, styrene, methyl methacrylate, isooctyl acrylate, butyl acrylate, acrylic acid, methacrylic acid, methacrylamide, lauryl sulfate Sodium, trimethylolpropane trimethacrylate, silica sol, sodium persulfate, organic peroxide, sodium binitrite, the contents of the above components are calculated in parts by mass: 80 parts of water, 30 parts of styrene , 20 parts of methyl methacrylate, 10 parts of isooctyl acrylate, 20 parts of butyl acrylate, 0.5 parts of acrylic acid, 0.5 parts of methacrylic acid, 1 part of methacrylamide, 5 parts of sodium lauryl sulfate, trihydroxy 1 part of methylpropane trimethacrylate, 0.5 part of silica sol, 0.2 part of sodium persulfate, 0.1 part of organic peroxide, and 0.1 part of sodium binitrite.
[0051] The preparation method of anti-fresh cement efflorescence primer styrene-acrylic emulsion of the present invention comprises the follo...
Embodiment 2
[0064] The anti-fresh cement efflorescence primer styrene-acrylic emulsion of the present invention comprises water, styrene, methyl methacrylate, isooctyl acrylate, butyl acrylate, acrylic acid, methacrylic acid, methacrylamide, lauryl sulfate Sodium, sodium dodecylbenzenesulfonate, trimethylolpropane trimethacrylate, trimethylolpropane acrylate, tripropylene glycol diacrylate, divinylbenzene, silica sol, aluminum sol, sodium persulfate , ammonium persulfate, potassium persulfate, organic peroxide, sodium binitrite, and vitamin C. The contents of the above components are calculated in parts by mass: 130 parts of water, 60 parts of styrene, and 80 parts of methyl methacrylate , 20 parts of isooctyl acrylate, 80 parts of butyl acrylate, 5 parts of acrylic acid, 5 parts of methacrylic acid, 5 parts of methacrylamide, 10 parts of sodium dodecyl sulfate, 10 parts of sodium dodecylbenzenesulfonate , 1 part of trimethylolpropane trimethacrylate, 1 part of trimethylolpropane acrylate...
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