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A kind of preparation method of foamed inorganic fiber fireproof insulation material

An inorganic fiber, fireproof and heat preservation technology, applied in the field of preparation of fireproof heat preservation materials, can solve the problems of low thermal conductivity, endanger personal safety, flammability, etc.

Active Publication Date: 2019-03-08
SHAANXI UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the thermal insulation materials used in China are mainly organic materials, which have a small thermal conductivity, but have the defect of being flammable. When burning, they will form drips and produce a large amount of toxic fumes, which endanger personal safety.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] The preparation method of the foamed inorganic fiber fireproof and thermal insulation material of the present invention comprises the following steps:

[0022] 1) Weigh the polyvinyl alcohol solution, sodium silicate solution and inorganic fiber, add the polyvinyl alcohol solution and sodium silicate solution into the flask, and adjust the pH value to 9, then stir under constant temperature conditions, and then sequentially Freeze and dissolve to obtain a mixture;

[0023] 2) adding the inorganic fibers to the mixture obtained in step 1) in batches, and stirring to disperse the inorganic fibers evenly, then removing the inorganic fibers, then placing the inorganic fibers in a mold, and then drying to obtain an inorganic fiber board;

[0024] 3) Weigh phenolic resin, melamine resin, ethanol, acid curing agent and diatomaceous earth, mix the phenolic resin and melamine resin, add ethanol to dilute, then add acid curing agent and diatomaceous earth, and then stir evenly to...

Embodiment 2

[0034] The preparation method of the foamed inorganic fiber fireproof and thermal insulation material of the present invention comprises the following steps:

[0035] 1) Weigh the polyvinyl alcohol solution, sodium silicate solution and inorganic fiber, add the polyvinyl alcohol solution and sodium silicate solution into the flask, and adjust the pH value to 8, then stir under constant temperature conditions, and then sequentially Freeze and dissolve to obtain a mixture;

[0036] 2) adding the inorganic fibers to the mixture obtained in step 1) in batches, and stirring to disperse the inorganic fibers evenly, then removing the inorganic fibers, then placing the inorganic fibers in a mold, and then drying to obtain an inorganic fiber board;

[0037] 3) Weigh phenolic resin, melamine resin, ethanol, acid curing agent and diatomaceous earth, mix the phenolic resin and melamine resin, add ethanol to dilute, then add acid curing agent and diatomaceous earth, and then stir evenly to...

Embodiment 3

[0047] The preparation method of the foamed inorganic fiber fireproof and thermal insulation material of the present invention comprises the following steps:

[0048] 1) Weigh the polyvinyl alcohol solution, sodium silicate solution and inorganic fiber, add the polyvinyl alcohol solution and sodium silicate solution into the flask, and adjust the pH value to 9, then stir under constant temperature conditions, and then sequentially Freeze and dissolve to obtain a mixture;

[0049] 2) adding the inorganic fibers to the mixture obtained in step 1) in batches, and stirring to disperse the inorganic fibers evenly, then removing the inorganic fibers, then placing the inorganic fibers in a mold, and then drying to obtain an inorganic fiber board;

[0050] 3) Weigh phenolic resin, melamine resin, ethanol, acid curing agent and diatomaceous earth, mix the phenolic resin and melamine resin, add ethanol to dilute, then add acid curing agent and diatomaceous earth, and then stir evenly to...

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PUM

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Abstract

The invention discloses a preparation method of a foaming inorganic fiber fireproof heat insulation material. The preparation method comprises the following steps of (1) adding a polyvinyl alcohol solution and a sodium silicate solution into a flask, adjusting the pH (potential of hydrogen) value, stirring at constant temperature, sequentially freezing and dissolving, so as to obtain a mixture; (2) adding the inorganic fiber into the mixture by batches, stirring, uniformly dispersing the inorganic fiber, fetching inorganic fiber, putting the inorganic fiber into a die, and drying, so as to obtain an inorganic fiber board; (3) mixing phenolic resin and melamine resin, adding ethyl alcohol to dilute, adding an acid curing agent and diatomite, and uniformly stirring, so as to obtain a fireproof impregnating liquid; (4) putting the inorganic fiber board into the fireproof impregnating liquid, and then putting the inorganic fiber board into an air ventilation environment to cure, so as to obtain the foaming inorganic fiber fireproof heat insulation material. The prepared foaming inorganic fiber fireproof heat insulation material has the advantages that the heat conduction coefficient is little, and the easiness in combustion is avoided.

Description

technical field [0001] The invention relates to a preparation method of a fireproof heat preservation material, in particular to a preparation method of a foamed inorganic fiber fireproof heat preservation material. Background technique [0002] Fly ash / coal gangue fiber is a new type of inorganic fiber that has come out in recent years. The fiber is made of solid waste obtained from industrial coal washing and coal burning, and is made through high-temperature melting, spinning, cooling and other processes. , Silencer, non-combustible, small thermal conductivity, light weight, etc., so it has broad development prospects. [0003] At present, the thermal insulation materials used in China are mainly organic materials. Such materials have low thermal conductivity, but have the defect of being flammable. When burning, they will form droplets and produce a large amount of toxic fumes, which endanger personal safety. Contents of the invention [0004] The purpose of the prese...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B28/26C04B111/28
CPCC04B28/26C04B2111/28C04B14/38C04B14/08C04B24/302C04B24/125C04B24/02C04B22/165C04B22/122
Inventor 苏秀霞钱进刘静张婧陈卓张姣苏俊宁张海宁
Owner SHAANXI UNIV OF SCI & TECH