Preparation method of iodic acid mixed solution and iodic acid mixed solution prepared by the method
A mixed solution and iodic acid technology, which is applied in botany equipment and methods, chemicals for biological control, animal husbandry, etc., can solve the problems of unfavorable iodic acid disinfection effect, influence, and influence on the stability of iodic acid mixed solution, etc. , to achieve excellent stability, convenient operation and low cost
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Embodiment 1
[0064] a) 2g of potassium iodide is dissolved in water to obtain an iodide solution;
[0065] b) Add 0.3g of concentrated sulfuric acid to 3g of pyridine, and stir for 15min; then add 5g of 30% hydrogen peroxide, keep stirring for 30min, and keep the temperature at 60°C; then, add 10g of n-octanol polyoxyethylene ether JFC, stir Uniformly; Then, add 3g refined iodine and iodide solution successively;
[0066] c) Add 24g of concentrated phosphoric acid, and stir for 15min; then, add 5.7g of concentrated sulfuric acid and water successively, continue stirring for 45min, stop stirring, and cool to obtain the iodic acid mixed solution of Example 1.
Embodiment 2
[0068] a) 3g of sodium iodide is dissolved in water to obtain an iodide solution;
[0069] b) Add 0.1g concentrated sulfuric acid to 5g coconut oil dimethylamine, and stir for 20min; then add 4g 30% hydrogen peroxide, keep stirring for 45min, the temperature of insulation is 60 ℃; then, add 13g fatty acid methyl ester polyester Oxyethylene ether, stir well; then, add 3.5g refined iodine and iodide solution successively;
[0070] c) Add 24g of concentrated phosphoric acid, and stir for 20min; then, add 5.9g of concentrated sulfuric acid and water successively, continue to stir for 45min, stop stirring, and cool to obtain the iodic acid mixed solution of Example 2.
Embodiment 3
[0072] a) 3g of potassium iodide is dissolved in water to obtain an iodide solution;
[0073] b) Add 0.4g of concentrated sulfuric acid to 4g of quinoline, and stir for 5-30min; then add 6g of 30% hydrogen peroxide, keep stirring for 50min, and keep the temperature at 70°C; then, add 7g of isooctyl alcohol polyoxyethylene ether JFC-2, stir evenly; then, add 2.5g refined iodine and iodide solution in sequence;
[0074] c) Add 30 g of concentrated phosphoric acid, and stir for 20 min; then, add 9.6 g of concentrated sulfuric acid and water successively, continue stirring for 45 min, stop stirring, and cool to obtain the iodic acid mixed solution of Example 3.
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