The present application relates to a kind of analytical methods for determining hydrogenation rate of hydrogenated
nitrile, comprising the following steps: using high-field nuclear magnetic or low-field nuclear magnetic, hydrogenated
nitrile sample containing
solvent is tested, setting sampling parameter, acquisition one-dimensional
nuclear magnetic resonance diffusion ordering spectrum spectrum diagram;Hydrogenated
nitrile corresponding
chemical shift and integral area information are obtained by one-dimensional
nuclear magnetic resonance diffusion ordering spectrum spectrum diagram, combined with nitrile
raw material component information, calculate hydrogenation rate;The nitrile
raw material component information includes
acrylonitrile content, 1,4-butadiene content, 1,2-butadiene content;Hydrogenated nitrile corresponding
chemical shift and integral area information include saturated
aliphatic hydrocarbon signal integral area, 1,4-butadiene CH=CH
signal and 1,2-butadiene CH=
signal integral area, 1,2-butadiene CH2= signal integral area.Compared with prior art, the present application is a kind of analytical methods for determining hydrogenation rate of hydrogenated nitrile containing
solvent, which can be used in nitrile
hydrogenation process, and hydrogenation rate is rapidly analyzed after
hydrogenation reaction.