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Piece-shaped temperature-regulating energy-storage phase-change fiber and preparation method thereof

An energy storage phase change, orange-lobed technology, applied in fiber processing, fiber chemical characteristics, rayon manufacturing, etc., can solve the problems of slow heat transfer, slow temperature regulation, and sensitivity needs to be further improved. Low, increase the speed, improve the effect of temperature regulation and insulation effect

Active Publication Date: 2020-04-14
WUHAN TEXTILE UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Conventional phase change fibers usually have shortcomings such as slow heat transfer and slow temperature adjustment rate. In order to improve similar problems, a Chinese invention patent application (application publication number: CN106801266A, application publication date: 2017-06-06) discloses phase change energy storage fibers The phase change energy storage fiber has a skin-core structure, the skin-core structure includes a skin layer and a core layer, the raw material of the skin layer is thermoplastic polymer, and the raw material of the core layer is a mixture of thermoplastic polymer, clay mineral powder and phase change material
The phase change energy storage fiber is a composite phase change material prepared by phase change material, clay mineral powder and thermoplastic polymer uniformly prepared to obtain a core layer raw material, and the core layer raw material is then compounded with a skin layer made of thermoplastic polymer The spinning machine is melt spun and spun into a phase change energy storage fiber with a skin-core structure. The phase change energy storage fiber with a skin-core structure of the present invention can prevent the leakage of the phase change material and improve the temperature adjustment rate to a certain extent. The disadvantages It is the sensitivity to temperature that needs to be further improved

Method used

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  • Piece-shaped temperature-regulating energy-storage phase-change fiber and preparation method thereof
  • Piece-shaped temperature-regulating energy-storage phase-change fiber and preparation method thereof
  • Piece-shaped temperature-regulating energy-storage phase-change fiber and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0043] 1) Preparation of thermally conductive masterbatch: use a large twin-screw extruder to mix thermally conductive powder alumina and polyester-polyethylene terephthalate (PET) at a mass ratio of 10:90 to prepare thermally conductive Masterbatch; the temperature values ​​of the large twin-screw extruder from left to right are 200°C, 220°C, 230°C, 240°C, 260°C, 270°C, 280°C, the speed of the main engine is 150r / min, and the feeding The speed is 28g / min;

[0044]2) Preparation of phase change masterbatch: use a beaker to hold 50g of attapulgite, place it in an ultrasonic instrument at 70°C for ultrasonic oscillation, then add 35g of octadecane solution dropwise, stir with a medicine spoon to make it evenly adsorbed, and continue to oscillate 30min, and then place it in a vacuum oven at 70°C for more than 12h to make it fully adsorbed to prepare a composite phase change material, and then combine the composite phase change material with polyester-polyethylene terephthalate (P...

Embodiment 2

[0054] 1) Preparation of thermally conductive masterbatch: use a large twin-screw extruder to prepare thermally conductive powder boron nitride and polyester-polyethylene terephthalate (PET) at a mass ratio of 10:90. Thermally conductive masterbatch; the temperature values ​​of the large twin-screw extruder from left to right are 200°C, 220°C, 230°C, 240°C, 260°C, 270°C, 280°C, and the speed of the main engine is 150r / min. The material speed is 28g / min;

[0055] 2) Preparation of phase change masterbatch: use a beaker to hold 50g of attapulgite, place it in an ultrasonic instrument at 70°C for ultrasonic oscillation, then add 35g of octadecane solution dropwise, stir with a medicine spoon to make it evenly adsorbed, and continue to oscillate 30min, and then place it in a vacuum oven at 70°C for more than 12h to make it fully adsorbed to prepare a composite phase change material, and then combine the composite phase change material with polyester-polyethylene terephthalate (PET...

Embodiment 3

[0062] 1) Preparation of thermally conductive masterbatch: use a large twin-screw extruder to prepare thermally conductive powder silicon carbide and polyester-polyethylene terephthalate (PET) at a mass ratio of 10:90 to obtain thermally conductive Masterbatch; the temperature values ​​of the large twin-screw extruder from left to right are 200°C, 220°C, 230°C, 240°C, 260°C, 270°C, 280°C, the speed of the main engine is 150r / min, and the feeding The speed is 28g / min;

[0063] 2) Preparation of phase change masterbatch: use a beaker to hold 50g of attapulgite, place it in an ultrasonic instrument at 70°C for ultrasonic oscillation, then add 35g of octadecane solution dropwise, stir with a medicine spoon to make it evenly adsorbed, and continue to oscillate 30min, and then place it in a vacuum oven at 70°C for more than 12h to make it fully adsorbed to prepare a composite phase change material, and then combine the composite phase change material with polyester-polyethylene tere...

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Abstract

The invention discloses an orange petal type temperature-regulating energy-storage phase change fiber and a preparation method thereof and belongs to the technical field of functional materials. The orange petal type temperature-regulating energy-storage phase change fiber is prepared from, by the same mass parts, a phase change component and a heat-conducting component in the mode that orange petal type composite spinning plates are arranged at intervals, wherein the phase change component is prepared from phase change master batch and a polymer, the mass ratio of the phase change master batch to the polymer is 10:90 to 30:70, the phase change component is obtained by blending inorganic powder absorbed with a phase change material and polyester, the heat-conducting component is prepared from heat-conducting master batch and a polymer, the mass ratio of the heat-conducting master batch to the polymer is 10:90 to 30:70, and the heat-conducting master batch is obtained by blending a heat-conducting material and polyester. The heat-conducting powder is added in the preparation process of the phase change fiber for solving the problem of low temperature-regulating speed of phase changefiber, the temperature sensitivity of the phase change fiber is improved, and the temperature-regulating speed of the phase change fiber is improved.

Description

technical field [0001] The invention relates to a segmented-pie-shaped temperature-regulating energy-storage fiber, which belongs to the technical field of functional materials, in particular to a segmented-pie-shaped temperature-regulating energy-storing phase-change fiber and a preparation method thereof. Background technique [0002] Phase change fiber is a kind of heat storage and temperature regulating functional fiber developed by utilizing the characteristics of releasing or absorbing latent heat and keeping temperature unchanged during the phase change of matter. In the process of phase transition, substances absorb and release energy to form their own microclimate. In this microclimate environment, the temperature is relatively constant and the external environment changes have little effect on it. Deeply affected by the energy crisis, reducing energy consumption and saving energy has become an urgent problem to be solved. The research on phase change fibers with te...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F6/92D01F6/90D01F6/46D01F1/10D01D5/253
CPCD01D5/253D01F1/10D01F6/46D01F6/90D01F6/92
Inventor 王栋牛应买赵青华梅涛毛秦岑罗宇郭启浩
Owner WUHAN TEXTILE UNIV
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