Low EFO polypropylene composition
A technology of polypropylene homopolymer and composition, applied in the field of new polymer composition, capable of solving problems such as poor FOG value
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[0084] Unless defined otherwise, the following definitions of terms and assay methods apply to the above general description of the invention as well as to the following examples.
[0085] 1. Measurement method
[0086] Quantification of microstructure by NMR spectroscopy
[0087] Quantitative nuclear magnetic resonance (NMR) spectroscopy was used to quantify the comonomer content of the polymers. Quantitation was recorded in solution state using a Bruker Advance III 400NMR spectrometer 13 C{ 1 H} NMR spectrum, for 1 H and 13 C, The spectrometers were operated at 400.15 MHz and 100.62 MHz, respectively. Using nitrogen for all pneumatics, all spectra were recorded at 125 °C using a 13C optimized 10 mm extended temperature probe. Mix approximately 200 mg of the material with chromium-(III) acetylacetonate (Cr(acac) 3 ) together in 3ml of 1,2-tetrachloroethane-d 2 (TCE-d 2 ), a 65 mM solution of the relaxant in the solvent was formed (as described in G. Singh, A. Kothari,...
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