Purifying agent for sulfur, arsenic and phosphorus and preparation method thereof
A purification agent, copper oxide technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of high bulk density and low adsorption capacity of purification agents
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Examples
Embodiment 1
[0037] 30 kg of copper nitrate trihydrate, 40 kg of zinc nitrate hexahydrate, 2 kg of iron nitrate, 2.5 kg of nickel nitrate hexahydrate and 500 kg of water were mixed and stirred evenly to obtain a metal salt solution, and 30 kg of sodium carbonate and 550 kg of water were mixed uniformly to obtain Sodium carbonate solution, mix sodium carbonate solution and metal salt solution evenly, react at 70°C for 1 hour, add 5 kg of pseudo-boehmite, react for 0.5 hour, wash the precipitate until the conductivity of the filtrate is less than 100 μs / cm, precipitate The material was dried, and then 1 kg of graphite and 30% by weight of water were added, mixed and rolled, granulated, roasted at 270° C. for 2 hours, and pressed into tablets. The composition of the obtained sample is shown in Table 1.
Embodiment 2
[0039] 20 kg of copper nitrate trihydrate, 50 kg of zinc nitrate hexahydrate, 2 kg of iron nitrate, 2.5 kg of nickel nitrate hexahydrate and 500 kg of water were mixed and stirred evenly to obtain a metal salt solution, and 30 kg of sodium carbonate and 550 kg of water were mixed uniformly to obtain Sodium carbonate solution, mix sodium carbonate solution and metal salt solution evenly, react at 60°C for 2 hours, add 5 kg of pseudo-boehmite, react for 0.5 hour, wash the precipitate until the conductivity of the filtrate is less than 100 μs / cm, and precipitate The material was dried, then 1 kg of graphite and 35% by weight of water were added, mixed and rolled, granulated, roasted at 270° C. for 2 hours, and pressed into tablets. The composition of the obtained sample was shown in Table 1.
Embodiment 3
[0041] 10 kg of copper nitrate trihydrate, 60 kg of zinc nitrate hexahydrate, 2 kg of iron nitrate, 2.5 kg of nickel nitrate hexahydrate and 500 kg of water were mixed and stirred evenly to obtain a metal salt solution, and 30 kg of sodium carbonate and 550 kg of water were mixed uniformly to obtain Sodium carbonate solution, mix sodium carbonate solution and metal salt solution evenly, react at 60°C for 2 hours, add 6 kg of pseudo-boehmite, react for 0.5 hour, wash the precipitate until the conductivity of the filtrate is less than 100 μs / cm, and precipitate The material was dried, then 1 kg of graphite and 35% by weight of water were added, mixed and rolled, granulated, roasted at 270° C. for 2 hours, and pressed into tablets. The composition of the obtained sample was shown in Table 1.
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Abstract
Description
Claims
Application Information
- IPC
- B01J20/06; B01J20/30
- CPC
- B01J20/02; B01J20/06
- Inventors
- 贾银娟; 王灿