This invention relates to the field of
electrosynthesis of high-value-added products, and more particularly to a supported catalyst for the electrocatalytic reduction of
oxygen to produce
hydrogen peroxide, its preparation method, and its application. The catalyst is represented by the formula NiTPP@CNT-ox, wherein
oxygen-
doped carbon nanotubes (CNT-ox) serve as the support, and
nickel tetraphenylporphyrin (NiTPP) serves as the
active site. This invention utilizes a dispersion-
adsorption method to adsorb NiTPP onto CNT-ox, obtaining the supported catalyst NiTPP@CNT-ox. The NiTPP@CNT-ox prepared by this invention exhibits high catalytic activity, selectivity, and excellent stability in the electrocatalytic reduction of
oxygen to produce
hydrogen peroxide, showing promising application prospects.