Normal-temperature desulfurization dearsenic agent and preparation method thereof
A technology of desulfurization and dearsenic, by weight, applied in separation methods, chemical instruments and methods, refining hydrocarbon oil, etc. The effect of increasing the chance of interface contact
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Embodiment 1
[0034] 30 kilograms of copper nitrate, 40 kilograms of zinc nitrate, 10 kilograms of aluminum nitrate, 1.0 kilogram of cerium nitrate and 500 kilograms of water are mixed and stirred to obtain a metal salt solution, and 30 kilograms of sodium carbonate and 550 kilograms of water are mixed to obtain a sodium carbonate solution. Mix the sodium solution and metal salt solution evenly, react at 70°C for 1 hour, wash and dry the precipitate, then add 6 kg of alumina and 1 kg of graphite, mix and roll, then add 30% by weight of water, granulate, and roast at 270°C After 2 hours, it was pressed into tablets and formed, and the composition of the obtained sample is shown in Table 1.
Embodiment 2
[0036] 30 kilograms of copper nitrate, 40 kilograms of zinc nitrate, 10 kilograms of aluminum nitrate, 0.02 kilogram of cerium nitrate and 500 kilograms of water are mixed and stirred to obtain a metal salt solution, and 30 kilograms of sodium carbonate and 550 kilograms of water are mixed to obtain a sodium carbonate solution. Mix the sodium solution and metal salt solution evenly, react at 70°C for 1 hour, wash and dry the precipitate, then add 6 kg of alumina and 1 kg of graphite, mix and roll, then add 30% by weight of water, granulate, and roast at 270°C After 2 hours, it was pressed into tablets and formed, and the composition of the obtained sample is shown in Table 1.
Embodiment 3
[0038] 30 kilograms of copper nitrate, 40 kilograms of zinc nitrate, 10 kilograms of aluminum nitrate, 0.1 kilogram of cerium nitrate and 500 kilograms of water are mixed and stirred to obtain a metal salt solution, and 30 kilograms of sodium carbonate and 550 kilograms of water are mixed to obtain a sodium carbonate solution. Mix the sodium solution and metal salt solution evenly, react at 70°C for 1 hour, wash and dry the precipitate, then add 6 kg of alumina and 1 kg of graphite, mix and roll, then add 30% by weight of water, granulate, and roast at 270°C After 2 hours, it was pressed into tablets and formed, and the composition of the obtained sample is shown in Table 1.
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