A kind of polyamide and its preparation method and application
A polyamide and caprolactam technology, applied in the petrochemical field, can solve the problems of affecting the relative molecular weight of the polymer product, poor compatibility, unfavorable polycondensation reaction, etc., and achieve the effects of improving the relative molecular mass, improving the elasticity index and reducing the cost.
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Embodiment 1
[0050] Add caprolactam, aerogel, surface modifier, acid anhydride, and initiator into a small amount of interface agent according to the ratio (parts by mass) shown in Table 1, heat at 100°C for 4.5 hours and stir thoroughly. The solvent was evaporated under reduced pressure and distilled off for recycling. Then discharge and dry to obtain Example 1.
Embodiment 2
[0052] According to the proportion of Example 2 shown in Table 1, the method of Example 1 was used to prepare polyamide.
Embodiment 3
[0062] Add the polyamide, polylactic acid, graft polymer and antioxidant obtained in Example 1 into the high-speed stirrer according to the formula in Table 3, the motor speed is 1300 rpm, take it out after mixing at room temperature for 2 minutes, and mix well The raw materials are put into the hopper of the Ф26 twin-screw extruder, and polylactic acid slices can be obtained after melting, extrusion, cooling and granulation.
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