Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Pyrophyllite synthetic block and its preparation method for solving the problem of synthetic diamond pressure relief and deflation gun

A technology for synthesizing diamonds and synthetic blocks, which is applied in the field of pyrophyllite synthetic blocks and its preparation, which can solve the problems of surrounding object hazards, diamond breaking, affecting diamond hardness, optical performance, etc., and achieve the effects of simplifying the process, saving time and manpower

Inactive Publication Date: 2021-05-04
TONGREN UNIV
View PDF11 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

According to the model of specific synthesis equipment and the market price of tungsten carbide anvil, the price of a tungsten carbide anvil is about 3000-18000 yuan, which will inevitably increase the cost of diamond industrialization
In addition, it will take a certain amount of time to replace the tungsten carbide anvil, which will delay the production or experiment cycle; (2) at the moment of deflation, the sudden drop (0.1-0.6GPa) in the internal pressure of the pyrophyllite block will cause diamond A large internal stress is generated instantly, which seriously affects the hardness and optical properties of the diamond, and even directly causes the diamond to be broken, and the broken diamond has low practical value; (3) at the moment of deflation, there will be small particles The material flying out will cause certain harm to the surrounding objects, and sometimes even cause personal safety

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Pyrophyllite synthetic block and its preparation method for solving the problem of synthetic diamond pressure relief and deflation gun
  • Pyrophyllite synthetic block and its preparation method for solving the problem of synthetic diamond pressure relief and deflation gun

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0018] The embodiment of the present invention provides a method for preparing pyrophyllite synthetic blocks for synthetic diamond pressure relief and deflation guns, including:

[0019] Analytical pure iron oxide (Fe 2 o 3 ) powder, since the iron oxide powder is difficult to be directly coated on the pyrophyllite composite block, therefore, the iron oxide powder is diluted with a diluent so that the iron oxide powder can be evenly coated on the pyrophyllite composite block. The purity of analytically pure iron oxide powder is not less than 99.7%, and superior pure iron oxide can also be selected. Considering cost and effect, analytically pure iron oxide is preferred.

[0020] The selection of the diluent should follow two principles: (1) The selected liquid should be chemically inert and cannot be mixed with pyrophyllite, tungsten carbide, Fe 2 o 3 etc.; (2) the selected liquid is volatile. Further, in a preferred embodiment of the present invention, the diluent includes...

Embodiment 1

[0027] This embodiment provides a synthetic block of pyrophyllite, which is mainly made by the following steps:

[0028] Select the particle size as 150 mesh to analyze pure iron oxide (Fe 2 o 3 ) powder 5g, dilute the iron oxide powder with 136g absolute ethanol, and fully stir evenly.

[0029] Fe with a soft brush 2 o 3 The powder mixture is evenly applied to the edges of the six sides of the pyrophyllite composite block according to the predetermined width, that is, the junction of two adjacent surfaces of the pyrophyllite composite block. Fe 2 o 3Width of powder coating=(side length of pyrophyllite synthetic block-side length of tungsten carbide atop hammer face) / 2.

[0030] The treated pyrophyllite composite block was dried at 90° C. for 40 minutes to ensure that the absolute ethanol was completely volatilized to obtain a pyrophyllite composite block coated with an iron oxide coating.

Embodiment 2

[0032] This embodiment provides a synthetic block of pyrophyllite, which is mainly made by the following steps:

[0033] Select the particle size as 220 mesh to analyze pure iron oxide (Fe 2 o 3 ) powder 5g, dilute the iron oxide powder with 144g absolute ethanol, and fully stir evenly.

[0034] Fe with a soft brush 2 o 3 The powder mixture is evenly applied to the edges of the six sides of the pyrophyllite composite block according to the predetermined width, that is, the junction of two adjacent surfaces of the pyrophyllite composite block. Fe 2 o 3 Width of powder coating=(side length of pyrophyllite synthetic block-side length of tungsten carbide atop hammer face) / 2.

[0035] Dry the treated pyrophyllite composite block at 110° C. for 20 minutes to ensure that all the diluent is volatilized to obtain a pyrophyllite composite block coated with an iron oxide coating.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
thicknessaaaaaaaaaa
particle size (mesh)aaaaaaaaaa
particle size (mesh)aaaaaaaaaa
Login to View More

Abstract

The invention provides a pyrophyllite synthetic block for synthesizing a diamond pressure relief and deflation gun and a preparation method thereof, and relates to the technical field of diamond synthesis. A method for preparing pyrophyllite synthetic blocks for synthetic diamond pressure relief and deflation guns, comprising mixing iron oxide powder with a diluent, applying the mixed solution to the edges of each face of the pyrophyllite synthetic blocks, and drying the treated pyrophyllite synthetic blocks , the iron oxide powder is attached to the edge of each surface of the pyrophyllite synthesis block with a predetermined width to form an iron oxide coating. The method is easy to operate, highly controllable, and suitable for large-scale production.

Description

technical field [0001] The invention relates to the technical field of diamond synthesis, and in particular relates to a pyrophyllite synthesis block for the synthesis of a diamond pressure relief and deflation gun and a preparation method thereof. Background technique [0002] Pyrophyllite is a kind of clay mineral with the chemical formula Al 2 (Si 4 o 10 )(OH) 2 , in view of its own excellent characteristics, it is often used as the peripheral material of the pressure transmission medium for high temperature and high pressure synthesis of diamond. In the process of high temperature and high pressure synthesis of diamond, the high pressure is generated by six carbide carbide anvils directly acting on the six surfaces of pyrophyllite and continuously extruded until the preset pressure value is reached, and then for The synthesis of diamond provides an ideal growth environment of static high pressure. When the diamond synthesis is over, it is generally used to stop heat...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): B01J3/06
CPCB01J3/06
Inventor 李勇廖江河宋谋胜佘彦超王强王应张志高
Owner TONGREN UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com