Cutting mechanism for blocky carbon tetrachloride precipitate
A carbon tetrachloride and sediment technology, which is applied in metal processing and other fields, can solve the problems of uneven mixing of mixed gas, limited operation efficiency, and high cost
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Embodiment 1
[0087] Prepare the refrigerant outlet pipe 5-9-9-5 of the present invention according to the following steps, and count in parts by weight:
[0088] Step 1: In an energy-saving stirred reactor, add 338.7 parts of purified water and 2-methyl-pentadecanoic acid-2-ethyl-2-[[(2-methyl-1-oxopentadecyl ) Oxygen] methyl generation] 130.6 parts of 1,3-propylene esters, start the stirrer in the energy-saving stirred reactor, set the rotating speed as 131rpm, start the steam coil heater in the energy-saving stirred reactor, make the temperature Rise to 146.7°C, add 133.8 parts of 4-methoxy-α-[[methylsulfonyl]oxy]imino]-phenylacetonitrile and stir evenly, react for 123.6 minutes, add 3-(methylthio)- 129.8 parts of butyraldehyde, the flow rate is 122.7m 3 Xenon gas per min for 123.6 minutes; then add 2.1 parts of Jinguanghong C13 to the energy-saving stirred reactor, start the steam coil heater in the energy-saving stirred reactor again, raise the temperature to 163.8°C, keep warm for 12...
Embodiment 2
[0095] Prepare the refrigerant outlet pipe 5-9-9-5 of the present invention according to the following steps, and count in parts by weight:
[0096] Step 1: In an energy-saving stirred reactor, add 563.8 parts of purified water and 2-methyl-pentadecanoic acid-2-ethyl-2-[[(2-methyl-1-oxopentadecyl ) Oxygen] methyl generation] 172.4 parts of 1,3-propylene esters, start the stirrer in the energy-saving stirred reactor, set the rotating speed as 177rpm, start the steam coil heater in the energy-saving stirred reactor, make the temperature Rise to 147.8°C, add 242.9 parts of 4-methoxy-α-[[methylsulfonyl]oxy]imino]-phenylacetonitrile and stir evenly, react for 134.4 minutes, add 3-(methylthio)- 146.3 parts of butyraldehyde, the flow rate is 163.3m 3 xenon gas per min for 134.4 minutes; then add 189.2 parts of Jinguanghong C to the energy-saving stirred reactor, start the steam coil heater in the energy-saving stirred reactor again, raise the temperature to 196.9°C, keep it warm for...
Embodiment 3
[0103] Prepare the refrigerant outlet pipe 5-9-9-5 of the present invention according to the following steps, and count in parts by weight:
[0104] Step 1: In an energy-saving stirred reactor, add 338.9 parts of purified water and 2-methyl-pentadecanoic acid-2-ethyl-2-[[(2-methyl-1-oxopentadecyl ) Oxygen] methyl generation] 130.9 parts of 1,3-propylene esters, start the stirrer in the energy-saving stirred reactor, set the rotating speed as 131rpm, start the steam coil heater in the energy-saving stirred reactor, make the temperature Rise to 146.9°C, add 133.9 parts of 4-methoxy-α-[[methylsulfonyl]oxy]imino]-phenylacetonitrile and stir evenly, react for 123.9 minutes, add 3-(methylthio)- 129.9 parts of butyraldehyde, the flow rate is 122.9m 3 xenon gas per min for 123.9 minutes; then add 2.9 parts of Jinguanghong C13 to the energy-saving stirred reactor, start the steam coil heater in the energy-saving stirred reactor again, raise the temperature to 163.9°C, keep the tempera...
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