Preparing method of high-thermal-stability VW93M nanometer magnesium alloy
A technology of high thermal stability and nano-magnesium, which is applied in the field of preparation of high-thermal-stability nano-magnesium alloys, can solve the problems of grain growth and poor thermal stability of nanostructured materials, and achieve the effect of increasing dislocation density
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Embodiment 1
[0015] The VW93M alloy bar was subjected to rotary forging deformation at 100°C, the amount of deformation in each pass was controlled to be 10%, 15%, and 15%, and the total deformation amount was 35%, and the feed rate was controlled to be 3mm / min. Change the feeding direction, oil lubrication is used in the swaging process, and the lubricant flow rate is 1m 3 / h, after swaging, anneal the obtained nano-magnesium alloy at 130°C for 20h.
[0016] The concentration of Gd and Y elements at the grain boundary of the obtained nano-magnesium alloy is 2.1 times that in the grain, and the grain growth temperature is 0.62T m .
Embodiment 2
[0018] The VW93M alloy bar was subjected to rotary forging deformation at 150°C, the deformation of each pass was controlled to be 10%, 15%, 10%, and 10%, the total deformation was 38%, and the feeding speed was controlled to be 5mm / min. Change the feeding direction after the first deformation, oil lubrication is used in the rotary forging process, and the lubricant flow rate is 1.5m 3 / h, the obtained nano-magnesium alloy was annealed at 150°C for 15h after swaging.
[0019] The concentration of Gd and Y elements at the grain boundary of the obtained nano-magnesium alloy is 2.3 times that in the grain, and the grain growth temperature is 0.63T m .
Embodiment 3
[0021] The VW93M alloy bar was subjected to rotary forging deformation at 200°C, the deformation of each pass was controlled to be 15%, 15%, 10%, and 10%, the total deformation was 41%, and the feed rate was controlled to be 6mm / min. Change the feeding direction after the first deformation, oil lubrication is used in the rotary forging process, and the lubricant flow rate is 1.5m 3 / h, after swaging, the nano-magnesium alloy was annealed at 140°C for 12h.
[0022] The concentration of Gd and Y elements at the grain boundary of the obtained nano-magnesium alloy is 2.5 times that in the grain, and the grain growth temperature is 0.62T m .
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