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A kind of rubber composition and vulcanized rubber and its preparation method and application

A rubber composition and polar rubber technology, applied in the rubber field, can solve the problems of insufficient mechanical properties, oil resistance and aging resistance, and achieve the effects of improving comprehensive performance, aging resistance and oil resistance.

Active Publication Date: 2021-07-02
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The object of the present invention is to provide a kind of rubber composition, a kind of preparation method of vulcanized rubber and the vulcanized rubber and its application

Method used

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  • A kind of rubber composition and vulcanized rubber and its preparation method and application
  • A kind of rubber composition and vulcanized rubber and its preparation method and application
  • A kind of rubber composition and vulcanized rubber and its preparation method and application

Examples

Experimental program
Comparison scheme
Effect test

Embodiment H1

[0073] (1) Prepare a rubber composition, the ingredients and parts by weight of the rubber composition are as shown in Table 1.

[0074] (2) The gained rubber composition is carried out banburying, and this banburying comprises first section banburying and second section banburying, specifically comprises:

[0075] The first stage of internal mixing: set the initial temperature of the internal mixer at 60±3°C, close the discharge port, fix the rotor, and raise the top bolt. Carry out the first batch of feeding according to the ingredients shown in Table 1: first add half of the polar rubber, then add the polar enhancer and coupling agent, and finally add the other half of the polar rubber; knead at 148°C for 5 minutes . Then raise the upper jacking bolt, add the second batch of materials according to the composition shown in Table 1, clean the top of the internal mixer inlet and the upper jacking bolt, and put down the upper jacking bolt; the control temperature is not higher...

Embodiment H2-H6

[0082] (1) Prepare a rubber composition, the ingredients and parts by weight of the rubber composition are as shown in Table 1.

[0083] (2) carry out banburying according to the method shown in embodiment H1. Wherein, according to a specific embodiment, in the mixed rubber material stage of the second stage banburying, when the temperature of the rubber material reaches 110° C. or reaches 5 minutes, the obtained mixed rubber can be unloaded if one of the conditions is met first.

[0084] The obtained mixed rubbers are respectively denoted as H2-H6.

Embodiment H7

[0086] (1) Prepare the same rubber composition as in Example H1.

[0087] (2) Banburying is carried out with reference to the step (2) of Example H1, the difference is that in the first section of banburying, the materials are not divided into two batches, but the materials of the first section of banburying are added at the same time.

[0088] The resulting compound was designated as H7.

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Abstract

The invention relates to the field of rubber, in particular to a rubber composition, a method for preparing vulcanized rubber, the vulcanized rubber prepared by the method and applications thereof. The rubber composition contains a polar rubber and a polar reinforcing agent, the polar rubber is composed of a polar structural unit and a non-polar structural unit, and the content of the polar structural unit is 25-45% by weight. The cohesive energy density of flexible rubber is 300‑400J / cm 3 ; The polar group density on the surface of the polarity enhancer is 0.1-10 groups / nm 2 , based on 100 parts by weight of the polar rubber, the content of the polar enhancer is 10-50 parts by weight. The vulcanized rubber of the invention can have good mechanical properties, compression deformation resistance, aging resistance and oil resistance.

Description

technical field [0001] The invention relates to the field of rubber, in particular to a rubber composition, a method for preparing vulcanized rubber, the vulcanized rubber prepared by the method and applications thereof. Background technique [0002] Rubber sealing parts are often used in high temperature, fuel and extremely harsh fluid environments, requiring vulcanized rubber to have good oil resistance, aging resistance and small compression set. However, most existing rubber products use a combination of non-polar rubber and non-polar reinforcing agent, such as butadiene rubber and carbon black. The oil resistance of the rubber product obtained by this combination is not ideal. Therefore, in order to make rubber products more suitable for rubber sealing parts, it is very important to study how to further improve oil resistance and maintain good mechanical properties and aging resistance. Contents of the invention [0003] The object of the present invention is to prov...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L9/02C08L15/00C08L11/00C08K13/02C08K3/36C08K3/04C08K5/09C08K3/22C08K5/11C08K5/12C08K5/14C08K5/18C08K5/47
CPCC08K3/04C08K3/22C08K3/36C08K5/09C08K5/11C08K5/12C08K5/14C08K5/18C08K5/47C08K13/02C08L2201/08C08L9/02C08L15/005C08L11/00
Inventor 赵青松解希铭王丽丽郑方远姜科王丽静唐功庆
Owner CHINA PETROLEUM & CHEM CORP