Preparation method of environment-friendly flexible lithium-ion battery positive electrode framework material
A lithium-ion battery and skeleton material technology, which is applied in the field of preparation of environmentally friendly flexible lithium-ion battery cathode skeleton materials, can solve the problems of limited reserves, long time required for the formation of fossil fuels, environmental pollution, etc.
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Embodiment 1
[0054]The preparation method comprises the following steps: providing polyurethane sponge; providing aniline monomer, sulfuric acid solution and ammonium persulfate; adding the aniline monomer into the sulfuric acid solution, and then adding ammonium persulfate into the mixed solution of sulfuric acid and aniline monomer to obtain the first mixed solution ; Add polyurethane sponge to the first mixed solution to obtain a second mixed solution; react the second mixed solution for 8 hours at 8°C and dry to obtain a modified polyurethane sponge; carbonize the modified polyurethane sponge to obtain carbonized Modified polyurethane sponge; aging the carbonized modified polyurethane sponge; configuring a graphene oxide solution; adding the aged carbonized modified polyurethane sponge into the graphene oxide solution and stirring and drying to obtain the modified polyurethane sponge / Graphene oxide composite material; heat treatment of modified polyurethane sponge / graphene oxide compos...
Embodiment 2
[0056] The preparation method comprises the following steps: providing polyurethane sponge; providing aniline monomer, sulfuric acid solution and ammonium persulfate; adding the aniline monomer into the sulfuric acid solution, and then adding ammonium persulfate into the mixed solution of sulfuric acid and aniline monomer to obtain the first mixed solution Add polyurethane sponge to the first mixed solution to obtain a second mixed solution; react the second mixed solution for 12 hours at 15°C and dry to obtain a modified polyurethane sponge; carbonize the modified polyurethane sponge to obtain carbonized Modified polyurethane sponge; aging the carbonized modified polyurethane sponge; configuring a graphene oxide solution; adding the aged carbonized modified polyurethane sponge into the graphene oxide solution and stirring and drying to obtain the modified polyurethane sponge / Graphene oxide composite material; heat treatment of modified polyurethane sponge / graphene oxide compo...
Embodiment 3
[0058] The preparation method comprises the following steps: providing polyurethane sponge; providing aniline monomer, sulfuric acid solution and ammonium persulfate; adding the aniline monomer into the sulfuric acid solution, and then adding ammonium persulfate into the mixed solution of sulfuric acid and aniline monomer to obtain the first mixed solution Add polyurethane sponge to the first mixed solution to obtain a second mixed solution; react the second mixed solution for 9 hours at 10°C and dry to obtain a modified polyurethane sponge; carbonize the modified polyurethane sponge to obtain carbonized Modified polyurethane sponge; aging the carbonized modified polyurethane sponge; configuring a graphene oxide solution; adding the aged carbonized modified polyurethane sponge into the graphene oxide solution and stirring and drying to obtain the modified polyurethane sponge / Graphene oxide composite material; heat treatment of modified polyurethane sponge / graphene oxide compos...
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