Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Phase-change composite material filled with nano-graphene sheet and preparation method thereof

A technology of phase-change composite materials and nano-graphene, which is applied in the direction of heat exchange materials, chemical instruments and methods, can solve the problem of low thermal conductivity of phase-change energy storage materials, and achieve the effect of improving thermal conductivity

Active Publication Date: 2021-04-13
CHONGQING UNIV
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention is to provide a phase-change composite material filled with nano-graphene sheets and a preparation method to solve the problem of low thermal conductivity of phase-change energy storage materials existing in the prior art

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Phase-change composite material filled with nano-graphene sheet and preparation method thereof
  • Phase-change composite material filled with nano-graphene sheet and preparation method thereof
  • Phase-change composite material filled with nano-graphene sheet and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0026] see figure 1 , the preparation method of the phase-change composite material that fills nano-graphene sheet, comprises the steps:

[0027] The first step: completely melt the n-octadecane solid that has been dried and pretreated;

[0028] The second step: adding the nano-graphene sheet and the hyperdispersant to the liquid phase n-octadecane in proportion to obtain a mixed suspension; the ratio of the nano-graphene sheet to n-octadecane is: 1:15~1: 200; the graphene nano sheet is a multi-layer structure with less than 20 layers. The hyperdispersant accounts for 0.1% of the total mass of the entire composite phase change material.

[0029] Step 3: Stir with a stirrer to mix the suspension evenly;

[0030] Step 4: Put the uniformly mixed suspension into an ultrasonic cleaning machine and oscillate ultrasonically to make the nano-graphene sheets form a stable three-dimensional heat-conducting network structure inside n-octadecane;

[0031] The fifth step: the suspensio...

Embodiment 1

[0034] The preparation method of the phase-change composite material filled with nano-graphene sheet, comprises the steps:

[0035] Step 1: Weigh 49.7g of dried and pretreated n-octadecane solid with an electronic balance and place it in a reagent bottle, move it to a constant temperature magnetic stirrer panel and heat until completely melted, and set the temperature to 65°C.

[0036] Step 2: After keeping the n-octadecane in a molten state for 30 minutes, add 0.25 g of graphene nanosheets and 0.05 g of hyperdispersant Disper S35 into the n-octadecane in liquid phase.

[0037] Step 3: first put the magnetic core into the reagent bottle, adjust the constant temperature magnetic stirrer to 450r / min, keep the temperature constant, and stir the composite phase change material suspension for 3 hours.

[0038] Step 4: Then take out the magnetic core, and place the reagent bottle in an ultrasonic cleaning machine for 30 minutes of ultrasonic vibration.

[0039] Step 5: Allow the su...

Embodiment 2

[0041] The preparation method of the phase-change composite material filled with nano-graphene sheet, comprises the steps:

[0042] Step 1: Weigh 49.2 g of dried and pretreated n-octadecane solid with an electronic balance and place it in a reagent bottle, move it to a constant temperature magnetic stirrer panel and heat until completely melted, and set the temperature to 65°C.

[0043] Step 2: After keeping the n-octadecane in a molten state for 30 minutes, add 0.75 g of nano-graphene sheets into the n-octadecane in liquid phase.

[0044] Step 3: first put the magnetic core into the reagent bottle, adjust the constant temperature magnetic stirrer to 450r / min, keep the temperature constant, and stir the composite phase change material suspension for 3 hours.

[0045] Step 4: Then take out the magnetic core, and place the reagent bottle in an ultrasonic cleaning machine for 30 minutes of ultrasonic vibration.

[0046]Step 5: Allow the suspension of the composite phase-change m...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
melting pointaaaaaaaaaa
solidification pointaaaaaaaaaa
solidification pointaaaaaaaaaa
Login to View More

Abstract

The invention discloses a phase-change composite material filled with nano-graphene sheets and a preparation method; the preparation method of the phase-change composite material filled with nano-graphene sheets is characterized in that it includes the following steps: the first step: drying and pre-treated The n-octadecane solid is completely melted; the second step: adding the nano-graphene sheet and the hyperdispersant to the liquid phase n-octadecane in proportion to obtain a mixed suspension; the third step: stirring with a stirrer to make the suspension The liquid is mixed evenly; the fourth step: put the uniformly mixed suspension into the ultrasonic cleaning machine, and ultrasonically vibrate, so that the nano-graphene sheet forms a stable three-dimensional heat conduction network structure inside the n-octadecane; the fifth step: put the fourth The suspension obtained in the first step is naturally cooled to solidification to obtain a phase-change composite material filled with n-octadecane as a matrix and filled with nano-graphene sheets; the present invention is widely used in fields such as energy.

Description

technical field [0001] The invention relates to a phase-change composite material, in particular to a phase-change composite material filled with nanographene sheets and a preparation method thereof. Background technique [0002] The phase change material absorbs or releases the latent heat of phase change during the phase change process, and is the medium for realizing phase change energy storage. Compared with sensible heat materials, phase change materials have a high density of latent heat storage, and can quickly absorb and release a large amount of heat under approximately constant temperature conditions. At the same time, phase change materials also have the advantages of suitable phase change temperature, small size, large phase change latent heat value, and easy control. However, phase change materials generally have the disadvantage of low thermal conductivity. Low thermal conductivity will lead to low conversion efficiency of the heat storage system of phase chan...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C09K5/06
CPCC09K5/063
Inventor 李静蔡迪焦乃勋李猛孙宽
Owner CHONGQING UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com