Silicone oil free and sulfate free shampoo with high conditioning performance and preparation method thereof
A silicone-free, sulfate-free technology, applied in medical preparations containing active ingredients, hair care, pharmaceutical formulas, etc., can solve difficult-to-care problems, achieve easy-to-care, avoid scalp problems, and have no risk of dioxane Effect
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[0050] In a specific embodiment, the present application provides a method for preparing a silicone oil-free and sulfate-free shampoo with high conditioning properties, which is characterized in that it comprises the following steps:
[0051] (1) Add water, sodium lauroyl sarcosinate, cocamidopropyl betaine, disodium EDTA, glyceryl laurate, and cocamidomethyl monoethanolamine in a stirring pot, and heat and stir;
[0052] (2) When the temperature is raised to 70°C, add polyquaternium-10, and stop heating after stirring evenly;
[0053] (3) When the temperature is lowered to 60°C, add PCA glycerol oleate, deep sea mustard oil, xylitol glucoside, anhydroxylitol and xylitol, and mix well;
[0054] (4) When the temperature is lowered to 45°C, add preservatives, flavors, and citric acid, and stop the stirring after uniformly stirring, to obtain the high-conditioning silicone oil-free and sulfate-free shampoo.
Example
[0069] Examples 1-3 and Comparative Examples 1-3
[0070] The preparation method of the silicone oil-free and sulfate-free shampoo of Examples 1-3 is as follows:
[0071] (1) Add water, sodium lauroyl sarcosinate, cocamidopropyl betaine, disodium EDTA, glyceryl laurate, and cocamidomethyl monoethanolamine in a stirring pot, and heat and stir;
[0072] (2) When the temperature is raised to 70°C, add polyquaternium-10, and stop heating after stirring evenly;
[0073] (3) When the temperature is lowered to 60℃, add PCA glycerol oleate, deep sea mustard oil, xylitol glucoside, anhydroxylitol and xylitol, and stir;
[0074] (4) When the temperature is lowered to 45°C, add preservatives, flavors, and citric acid, and stop the stirring after uniformly stirring, to obtain the high-conditioning silicone oil-free and sulfate-free shampoo.
[0075] The formulations of Examples 1-3 and Comparative Examples 1-3 are shown in Table 1.
Example Embodiment
[0080] Example 4 Evaluation of hair combing performance test:
[0081] Experimental equipment: INSTRON static carding machine
[0082] testing method:
[0083] All natural untreated Asian hair strands to be tested were first washed with Comparative Example 1 until they were foam-free, and the wet combing and dry combing test was performed on the INSTRON static combing machine. Then, the shampoos of Example 1-3 and Comparative Example 2-3 were used for washing and wet combing test; after the hair tress was naturally dried at room temperature 25° C. and humidity 60%, the dry combing test was performed. According to the dry and wet hair combing work twice before and after each hair tress, the improvement rate of dry and wet hair combability is calculated.
[0084] Table 2 lists the hair combing force test data of Examples 1-3, Comparative Examples 1-3 and a commercially available shampoo. This commercially available shampoo is Head & Shoulders anti-dandruff shampoo containing silicone ...
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