Hydrophobic easy-to-clean powder coating
A powder coating, easy-to-clean technology, applied in the field of coatings, can solve the problems of high raw material cost, unfavorable industrial application, and decreased product surface cleanliness
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[0027] Example 1:
[0028] (1) The preparation process of organosilane modified saturated hydroxyl terminated polyester resin is as follows:
[0029] ① Mixing of raw materials: add 353g isophthalic acid, 147g ethylene glycol, 100g hydroxy silicone oil and 400g xylene into the reaction vessel, raise the temperature to 100°C, and wait for the materials to dissolve;
[0030] ②Polymerization reaction: After stirring the reaction system to 180°C, add 0.5g of tetrabutyl titanate dropwise to the reaction vessel under the protection of nitrogen, and carry out the polymerization reaction for 2h while keeping warm;
[0031] ③Post-treatment: use normal pressure and reduced pressure distillation to remove the solvent, pour the material into an aluminum pan while it is hot, cool and pulverize to obtain the organic silicon modified saturated hydroxyl-terminated polyester resin of the present invention. The hydroxyl value is measured It is 37mgKOH / g.
[0032] (2) A high-toughness super weather-resist...
Example Embodiment
[0045] Example 2:
[0046] (1) The preparation process of organosilane modified saturated hydroxyl terminated polyester resin is as follows:
[0047] ① Mixing of raw materials: add 347g of succinic acid, 243g of 1,2-propanediol, 150g of hydroxysilicone oil and 250g of xylene into the reaction vessel, raise the temperature to 110°C, and wait until all the materials are dissolved;
[0048] ②Polymerization reaction: After stirring the reaction system to 190°C, add the catalyst dropwise to the reaction vessel under the protection of nitrogen, and keep it warm for 2.5h;
[0049] ③Post-treatment: use normal pressure and reduced pressure distillation to remove the solvent, pour the material into an aluminum pan while it is hot, cool and pulverize, to obtain the organic silicon modified saturated hydroxyl-terminated polyester resin of the present invention, and the hydroxyl value is measured It is 52mgKOH / g.
[0050] (2) A self-cleaning powder coating, including the following components by wei...
Example Embodiment
[0063] Example 3:
[0064] (1) The preparation process of organosilane modified saturated hydroxyl terminated polyester resin is as follows:
[0065] ① Mixing of raw materials: add 372g of glutaric acid, 328g of neopentyl glycol, 200g of hydroxy silicone oil and 100g of xylene into the reaction vessel, raise the temperature to 120°C, and wait until all the materials are dissolved;
[0066] ②Polymerization reaction: After stirring the reaction system to 210°C, add the catalyst dropwise to the reaction vessel under the protection of nitrogen, and keep it warm for 3h;
[0067] ③Post-treatment: use normal pressure and reduced pressure distillation to remove the solvent, pour the material into an aluminum pan while it is hot, cool and pulverize, to obtain the organic silicon modified saturated hydroxyl-terminated polyester resin of the present invention, and the hydroxyl value is measured It is 42mgKOH / g.
[0068] (2) A self-cleaning powder coating, including the following components by wei...
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