A kind of method that utilizes high-concentration starch milk to continuously produce starch saccharification product

A starch milk and starch sugar technology, applied in biochemical equipment and methods, glycosylases, glycosyltransferases, etc., can solve the problems of glucose compound reaction, complex processing, increased viscosity, etc., to achieve continuous production, inhibit Compound reaction, fast filtration effect

Active Publication Date: 2019-12-17
JILIN COFCO BIOCHEM +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, at the above temperature, the gelatinization of starch is still very serious, and the limitation of viscosity on the process is still very obvious, so it is usually difficult to increase the initial concentration of starch milk to more than 35%.
On the other hand, when indirect heating is used, the starch is heated for too long, resulting in a high viscosity of the liquefied liquid, which complicates pumping and subsequent processing
[0004] In the enzymatic hydrolysis sugar production process, the increase of the initial concentration of starch milk will lead to the following two technical problems: 1) In the liquefaction stage, the viscosity of high-concentration starch will increase sharply during the heating and gelatinization process, making liquefaction control become difficult. 2) During the saccharification stage, the increase of the substrate concentration will cause the compound reaction of glucose to generate a large amount of disaccharides and trisaccharides, thereby reducing the yield of glucose
[0005] However, in the late sugar solution evaporation process of starch sugar production, the concentration of the saccharification solution needs to be concentrated (for example, to 45%), and the lower initial concentration range of starch milk cannot overcome the disadvantages caused by the evaporation of the sugar solution in the later stage of starch sugar production. Problems such as high energy consumption and high water consumption

Method used

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  • A kind of method that utilizes high-concentration starch milk to continuously produce starch saccharification product
  • A kind of method that utilizes high-concentration starch milk to continuously produce starch saccharification product
  • A kind of method that utilizes high-concentration starch milk to continuously produce starch saccharification product

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Effect test

Embodiment 1- Embodiment 4

[0097] Embodiment 1-Example 4: Utilize high-concentration starch milk to produce starch saccharification product

Embodiment 1

[0099] (1) Pre-liquefaction step: using commercially available cornstarch as a raw material, prepare starch milk with a dry basis mass fraction of 45wt% in a mixing tank at 50°C, adjust the pH to 6.0 with 8M hydrochloric acid, dry the starch milk with starch milk Based on the starch milk in the mixing tank, add 0.15wt‰ of medium temperature α-amylase, 0.2wt‰ of high temperature resistant α-amylase, 0.04wt‰ of lipase and 0.07wt‰ of neutral protease, After mixing, heat preservation at 55° C. for 0.5 h to obtain the first starch milk with a brix value of 15%.

[0100] (2) Liquefaction step: at 0.18m 3 The speed of / h causes the first starch milk to be discharged from the mixing tank through the pipeline into the spray gun, sprayed out through the spray gun mouth and contacted with high-pressure steam (the pressure is 0.6MPa) to carry out spray liquefaction, and the temperature of the spray gun mouth is 108 ° C; The sprayed liquefied material is kept in the maintenance tube for 3...

Embodiment 2

[0104] (1) Pre-liquefaction step: using commercially available cornstarch as a raw material, starch milk with a mass fraction of 40 wt% on a dry basis was prepared in a mixing tank at 50°C, and the pH was adjusted to 6.0 with 8M hydrochloric acid. Based on the starch dry basis of starch milk, add 0.2wt‰ of medium temperature α-amylase, 0.2wt‰ of high temperature resistant α-amylase, 0.08wt‰ of lipase and 0.12wt‰ of Protease, mixed and incubated at 55°C for 0.5h to obtain the first starch milk with a brix value of 13%.

[0105] (2) Liquefaction step: at 0.18m 3 The first starch milk is discharged from the mixing tank through the pipeline at a speed of / h into the spray gun, sprayed out through the spray gun mouth and contacted with high-pressure steam (the pressure is 0.6MPa) to carry out jet liquefaction, and the temperature of the spray gun mouth is 108 ° C; The sprayed liquefied material is kept in the maintenance tube for 3 minutes, and then enters the flash tank for flash...

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Abstract

The present invention provides a method for continuously producing starch saccharification products by utilizing high-concentration starch milk. The method uses a combination of medium-temperature amylase, high-temperature amylase, lipase and protease in a pre-liquefaction step, and implements a two-step pre-liquefaction step. Then, continuous spray liquefaction is carried out, which effectively reduces the viscosity of starch in the process of heating and gelatinization, so that high-concentration starch milk can be better liquefied by spray liquefaction. In addition, the method uses an efficient complex saccharification enzyme that removes glucosidase as an enzyme preparation in the saccharification step, which effectively inhibits the occurrence of complex reactions in the saccharification stage, ensures the yield of glucose in the starch saccharification product, and thus achieves starch saccharification. Balance of energy reduction, viscosity control and glucose yield in the production of saccharified products.

Description

technical field [0001] The invention belongs to the technical field of starch sugar processing, and in particular relates to a method for continuously producing starch saccharification products using high-concentration starch milk. Background technique [0002] Starch sugar is a general term for sugar products obtained from starch as raw material by enzymatic hydrolysis sugar production process or acid sugar production process. Starch sugar is an important raw material of my country's food industry and a beneficial supplement for people's daily consumption of sugar. Therefore, it is particularly important to improve the quality of starch sugar products and reduce production costs. In recent years, the enzymatic hydrolysis sugar production process has gradually replaced the acid sugar production process. Generally speaking, the enzymatic hydrolysis sugar production process is generally divided into two stages: liquefaction and saccharification: firstly, the starch milk is li...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C12P19/16C12P19/14C12P19/02
CPCC12P19/02C12P19/14C12P19/16C12Y302/01001C12Y302/01003C12Y302/01041C12Y204/01024
Inventor 佟毅刘安妮李义丁子元刘颖慰吴延东曹雪邓莉川陶进
Owner JILIN COFCO BIOCHEM
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