Antioxidant and whitening composition for skins and preparation method thereof
An anti-oxidation and composition technology is applied in the field of skin anti-oxidation and whitening compositions and the preparation thereof, which can solve the problems of low sunscreen effect and complicated use process of sunscreen skin care products, and achieves improved sunscreen performance, improved effect, and efficient dissolution and dispersion. performance effect
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Embodiment 1
[0022] The concrete preparation process of sunscreen whitening agent is as follows:
[0023] Step 1: Add 100g of p-methoxycinnamic acid into 700mL of thionyl chloride, raise the temperature to 60-70°C and stir for 5-6h, then distill to remove unreacted thionyl chloride to obtain p-methoxy Cinnamoyl chloride;
[0024] Step 2: Add 214g of p-methoxycinnamoyl chloride prepared in step 1 to 1200mL of pyridine, and at the same time add 83.6g of glycolic acid to it and raise the temperature to 70-80°C for reflux reaction for 8-9h, then cool to room temperature and crystals precipitate out. The precipitated crystals are washed and dried to obtain product A;
[0025] Step 3: two constant-pressure dropping funnels are installed in the four-necked flask, and the product A prepared in 455.5g step 2 and 168.7g p-hydroxyphenylacetic acid are added respectively in the ethanol solution to be configured as a 50% solution, and then Add the configured product A solution and p-hydroxyphenylacet...
Embodiment 2
[0028]The concrete preparation process of sunscreen whitening agent is as follows:
[0029] Step 1: Add 100g of p-methoxycinnamic acid into 700mL of thionyl chloride, raise the temperature to 60-70°C and stir for 5-6h, then distill to remove unreacted thionyl chloride to obtain p-methoxy Cinnamoyl chloride;
[0030] Step 2: Add 214g of p-methoxycinnamoyl chloride prepared in step 1 to 1200mL of pyridine, and at the same time add 83.6g of glycolic acid to it and raise the temperature to 70-80°C for reflux reaction for 8-9h, then cool to room temperature and crystals precipitate out. The precipitated crystals are washed and dried to obtain product A;
[0031] Step 3: two constant-pressure dropping funnels are installed in the four-necked flask, and the product A prepared in 236g step 2 and 337g p-hydroxyphenylacetic acid are added respectively in the ethanol solution to be configured into a 50% solution, and then the configured The product A solution and p-hydroxyphenylacetic ...
Embodiment 3
[0033] A preparation method of a skin antioxidant whitening composition, the specific preparation process is as follows: 11g of stearic acid, 2.4g of lauryl alcohol, 1.5g of triethanolamine, 4.3g of the sunscreen whitening agent prepared in Example 1 and 6.2g of Example 1 were prepared Add the bacteriostatic antioxidant of the above-mentioned 63g water, and then heat it to 50-55° C. and stir and mix quickly, then stir the mixed solution in a beater for 20-30 minutes and then gradually cool it down to obtain an anti-oxidation whitening composition.
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