The invention relates to a technology for detecting
chlorobenzene compounds and particularly relates to a method for determining the
chlorobenzene compounds in a plastic product. The method comprises the following steps: (1)
sample preparation: selecting samples and crushing the samples into uniform samples with a
high polymer material sample
crusher; (2) extraction: adding the samples into a
solvent, tightly plugging, extracting in a
microwave extractor, filtering extract liquor, blowing with
nitrogen and waiting for purification; (3) purification: activating a PA (
polyamide) pillared with a
solvent, adding the samples into the
solvent for
dissolution, eluting with the solvent, blowing to be dry with
nitrogen and metering volume with propyl
alcohol; (4) gaschromatographic
mass spectrometric determination: respectively absorbing a to-be-determined
standard solution and a to-be-determined sample solution, injecting a gaschromatographic
mass spectrometer for determining and finally calculating the content of
chlorobenzene compounds in the samples. The determination method provided by the invention has the advantages that 12 types of chlorobenzene organic compounds in plastics can be simultaneously detected, therefore, the sensitivity is relatively high, the limit of detection is low, the
degree of precision is good, the detection period is short, the anti-interference capacity is strong, and the method is fast, stable and accurate.