Rapid test strip for chloramphenicol drug residue
A technology for detecting test strips and chloramphenicol, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of complicated operation, difficult to popularize, expensive equipment, etc. easy effect
Patent Information
- Authority / Receiving Office
- CN · China
- Current Assignee / Owner
- Publication Date
- 2019-05-28
- Estimated Expiration
- Not applicable · inactive patent
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Abstract
Description
technical field
[0001] The invention relates to a rapid detection test strip for detecting chloramphenicol drug residues, belonging to the field of rapid detection of food safety. technical background
[0002] Chloramphenicol is a broad-spectrum antibiotic, commonly used in the treatment of various infectious diseases in animals, and has a strong inhibitory effect on a variety of pathogenic bacteria. Chloramphenicol has serious side effects, which can inhibit the hematopoietic function of human bone marrow and cause human aplastic anemia and other diseases. Therefore, chloramphenicol residues in animal food pose a huge threat to human health.
[0003] At present, the determination methods of chloramphenicol and its metabolites in food of animal origin are mainly physical and chemical detection methods. For example, chemical analysis is used to determine the residual amount of chloramphenicol in shrimp meat, and the detection limit is 0.0125ug / kg. Determination of chloramphe...
Examples
Embodiment Construction
[0018] To prepare test strips for rapid detection of chloramphenicol residues, it is first necessary to prepare the carrier protein and gold-labeled antibody coupled to chloramphenicol drug, so as to prepare the detection blot and gold-labeled antibody fiber; secondly, it is necessary to prepare goat anti or rabbit anti-mouse IgG Antibodies, used to prepare control blots.
[0019] 1. Conjugation of Chloramphenicol Drug to Carrier Protein
[0020] Coupling of chloramphenicol with ovalbumin and hemocyanin by mixed anhydride method and carbodiimide method respectively to obtain coating agent (for immobilization on reaction membrane) and immunogen (for preparation of monoclonal antibody) .
[0021] (1) Preparation of the original coating:
[0022] ①Dissolve 5mg of chloramphenicol in 0.5mL formamide (DMF), cool to 10°C, add 5 μl of isobutyl chloroformate, and stir for 30 minutes at 4°C to obtain the reaction solution Ⅰ;
[0023] ② Weigh 30 mg of ovalbumin (OVA), and dissolve it ...