Mushroom head type electrostatic spinning sprayer with controllable free liquid level suitable for high-speed motion and using method of mushroom head type electrostatic spinning sprayer
An electrospinning, high-speed motion technology, applied in textile and papermaking, filament/thread forming, fiber processing, etc., can solve the problem of unstable free liquid surface, volatile solvent of spinning solution, Problems such as excessive free liquid level, to achieve the effect of simple and easy technology and reducing solvent volatilization
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Embodiment 1
[0049] Next, nanofibers are prepared by using a polymer solution prepared from polyacrylonitrile (PAN) and N-N dimethylformamide (DMF). The mass fraction of the prepared PAN polymer solution is 10%. The metal drum 10 is grounded, and the distance between the metal cylindrical drum 10 and the controllable free-surface mushroom head type electrospinning nozzle suitable for high-speed motion is 20 cm; The relative height forms the ring-shaped slit channel 14 of certain width to be 0.5mm; Turn on the drive motor 9 of the metal cylindrical cylinder 10 of the receiving device, and set the rotating speed of the cylinder 10 to be 60r / min; Open the switch of the liquid supply control device 16, through the peristaltic pump to Inject a certain amount of high polymer spinning solution 1 into the annular slit channel 14 until the surface solution is completely full; set the reciprocating speed of the mushroom-head type electrospinning nozzle suitable for high-speed movement to a controlla...
Embodiment 2
[0051] This embodiment is similar to Embodiment 1, except that: the mass fraction of the prepared PAN polymer solution is 12%; the metal cylindrical drum 10 and the controllable free liquid surface mushroom head type electrospinning nozzle suitable for high-speed motion The distance of the spinning solution is adjusted to 18cm; the ring-shaped slit channel 14 of a certain width formed between the spinning solution curvature control module 13 and the polytetrafluoroethylene seat 2 is 0.6mm; the rotating speed of the drum 10 is set to 80r / min; suitable for high-speed motion The reciprocating speed of the mushroom-head electrospinning nozzle with controllable free liquid surface is set to 1200mm / s; the voltage of switch 4 of the high voltage generator is adjusted to 80KV.
Embodiment 3
[0053] This embodiment is similar to Embodiment 1, except that: the mass fraction of the prepared PAN polymer solution is 14%; the metal cylindrical drum 10 and the controllable free surface mushroom head type electrospinning nozzle suitable for high-speed motion The distance is adjusted to 25cm; the ring-shaped slit channel 14 of a certain width formed between the spinning solution curvature control module 13 and the polytetrafluoroethylene seat 2 is 0.7mm; the rotating speed of the drum 10 is set to 90r / min; suitable for high-speed motion The reciprocating speed of the mushroom head electrospinning nozzle with controllable free liquid surface was set to 1500mm / s.
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