Preparation method of aerogel-based photocatalytic material
A technology of photocatalytic materials and airgel, which is applied in the direction of catalyst activation/preparation, chemical instruments and methods, separation methods, etc., can solve the problems of low photocatalytic efficiency, small visible light response, and low solar energy utilization efficiency, and achieve photocatalytic The effect of improving efficiency
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[0024]Add 50-60mL absolute ethanol into 6-8mL tetraethyl orthosilicate along the wall of the beaker, stir for 10-15min, add 3-4mL water into the beaker, stir for 10-12min, then add 15 % hydrochloric acid to adjust the pH of the solution in the beaker to 1.8-2.2, and let it stand for 3-4 hours to obtain a silica sol for later use; Add 18-20mL tetrabutyl titanate into the three-necked flask at a dropping rate of 2-3mL / min from the dropping funnel, start the stirrer at the same time, start stirring at a speed of 200-300r / min, and add tetrabutyl titanate dropwise After completion, add 4-6mL triethanolamine to the three-necked flask and stir for 1-2 hours to obtain a uniform solution; mix 1-2mL water, 8-10mL absolute ethanol, and 2-4mL hydrochloric acid with a mass fraction of 20%, pour into In the above-mentioned three-necked flask, continue to stir and mix for 2-3 hours, and then let it stand for 5-6 hours to obtain a light yellow titanium dioxide sol, and then add 1-3 mL of poly...
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