A dyeing and finishing method for improving the color fastness of fabrics
A color fastness and fabric technology, applied in dyeing, textiles and papermaking, etc., can solve the problems of affecting the appearance of clothes, fading, and affecting appearance, and achieve the effect of improving anti-ultraviolet radiation performance, improving bonding strength, and preventing ultraviolet rays
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Embodiment 1
[0018] The specific preparation process of color-fixing finishing agent is as follows:
[0019] Step 1: Add 13.6g of p-hydroxyacetophenone into 163g of 70-80°C hot water and stir to dissolve, then keep the temperature constant and add 8.1g of formaldehyde solution with a mass concentration of 37% and stir evenly, then adjust the concentration of the solution with hydrochloric acid pH=1, dropwise add 5.04g of concentrated ammonia water dropwise, stir vigorously while adding dropwise, control the drop rate to be 6-7mL / min, keep constant temperature reaction for 5-6h after dropwise addition is complete, then carry out vacuum distillation to obtain White powder;
[0020] Step 2: Add 10g of the white powder prepared in step 1 into 150mL of ethanol and stir to dissolve, then add 16.8g of epichlorohydrin to it, heat up to 75°C, and add 3.2g of 50% hydrogen hydroxide to the reaction vessel Sodium solution, constant temperature reflux, stirring and reacting for 12 hours, then evaporat...
Embodiment 2
[0023] The specific preparation process of color-fixing finishing agent is as follows:
[0024] Step 1: Add 9.06g of p-hydroxyacetophenone into 163g of 70-80°C hot water and stir to dissolve, then keep the temperature constant and add 5.4g of formaldehyde solution with a mass concentration of 37% and stir evenly, then adjust the concentration of the solution with hydrochloric acid pH=1, dropwise add 5.04g of concentrated ammonia water dropwise, stir vigorously while adding dropwise, control the drop rate to be 6-7mL / min, keep constant temperature reaction for 5-6h after dropwise addition is complete, then carry out vacuum distillation to obtain White powder;
[0025] Step 2: Add 10g of the white powder prepared in step 1 into 150mL of ethanol and stir to dissolve, then add 16.8g of epichlorohydrin to it, heat up to 75°C, and add 3.2g of 50% hydrogen hydroxide to the reaction vessel Sodium solution, constant temperature reflux, stirring and reacting for 12 hours, then evaporat...
Embodiment 3
[0028] The specific preparation process of color-fixing finishing agent is as follows:
[0029]Step 1: Add 13.6g of p-hydroxyacetophenone into 163g of 70-80°C hot water and stir to dissolve, then keep the temperature constant and add 8.1g of formaldehyde solution with a mass concentration of 37% and stir evenly, then adjust the concentration of the solution with hydrochloric acid pH=1, dropwise add 5.04g of concentrated ammonia water dropwise, stir vigorously while adding dropwise, control the drop rate to be 6-7mL / min, keep constant temperature reaction for 5-6h after dropwise addition is complete, then carry out vacuum distillation to obtain White powder;
[0030] Step 2: Add 10g of the white powder prepared in step 1 into 150mL of ethanol and stir to dissolve, then add 16.8g of epichlorohydrin to it, heat up to 75°C, and add 3.2g of 50% hydrogen hydroxide to the reaction vessel Sodium solution, constant temperature reflux, stirring and reacting for 12 hours, then evaporate...
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