One-stage serial hydrocracking process

A hydrocracking and hydrofining technology, which is applied in the fields of hydrotreating process, hydrocarbon oil treatment products, hydrocarbon oil treatment, etc., can solve the problems of low economic benefit, limited yield of chemical raw materials, low improvement of jet fuel quality, etc.

Active Publication Date: 2021-10-08
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method organically combines the high temperature and high pressure counter-current heat transfer technology with the hydrocracking catalyst grading technology, comprehensively utilizes the heat of hydrocracking reaction, and not only fully utilizes the characteristics of two different types of hydrocracking catalysts, but also maintains catalyst selectivity. Improve the quality of the target product, and reduce the project investment and operating energy consumption. This method has a limited yield of chemical raw materials, and the improvement rate of jet fuel quality is low, and the economic benefit is low.

Method used

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  • One-stage serial hydrocracking process
  • One-stage serial hydrocracking process
  • One-stage serial hydrocracking process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] Using raw oil 1 as the raw material, two catalyst beds are set in the hydrofinishing reactor, and three catalyst beds are set in the hydrocracking reactor. Catalyst I, catalyst II and catalyst III are loaded sequentially along the flow direction, and the catalyst loading volume ratio is 1:1:1. See Tables 4 and 5 for specific hydrogenation reaction conditions, product distribution and properties.

Embodiment 2

[0045] Same as Example 1, 2 catalyst beds are set in the hydrofinishing reactor, and 3 catalyst beds are set in the hydrocracking reactor, the difference is that the catalyst loading volume ratio is 2:1:1. See Tables 4 and 5 for specific hydrogenation reaction conditions, product distribution and properties.

Embodiment 3

[0047] Same as Example 1, 2 catalyst beds are set in the hydrofinishing reactor, and 3 catalyst beds are set in the hydrocracking reactor, the difference is that the catalyst loading volume ratio is 1:2:1. See Tables 4 and 5 for specific hydrogenation reaction conditions, product distribution and properties.

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Abstract

The invention discloses a one-stage serial hydrocracking method, which includes the following contents: (1) The raw material of wax oil is mixed with hydrogen and first enters a hydrorefining reactor for desulfurization, denitrogenation and aromatic hydrocarbon saturation reaction; (2) Step (1) The effluent enters the hydrocracking reactor, and the hydrocracking reactor includes the first to nth catalyst beds along the material direction, wherein n≥3, and each catalyst bed is filled with hydrocracking catalysts with different contents of modified Y molecular sieves; (3) The effluent from the hydrocracking reactor undergoes gas-liquid separation and liquid phase fractionation to obtain naphtha, jet fuel and diesel products. The method uses wax oil as a raw material, increases the production of heavy naphtha with high aromatic potential, and improves the quality of jet fuel and diesel products by setting a reasonable catalyst gradation mode and adjusting the catalyst composition and structure in the gradation bed layer.

Description

technical field [0001] The invention relates to a hydrocracking method, in particular to a hydrocracking method for producing high-quality clean fuel by using vacuum wax oil as a raw material. Background technique [0002] Hydrocracking technology has the characteristics of strong adaptability to raw materials, great flexibility in production operations and product plans, and good product quality. It can directly convert various heavy and low-quality feedstocks into high-quality jet fuel, diesel, and lubricating oil base materials that are urgently needed by the market. As well as chemical naphtha and tail oil steam cracking raw materials for ethylene production, it has become one of the most important heavy oil deep processing processes in modern oil refining and petrochemical industries, and has been increasingly widely used at home and abroad. [0003] CN200610008413.X discloses a combined hydrocracking method. In this method, low-quality catalytic cracking diesel oil is ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10G67/02
CPCC10G67/02C10G2300/1037C10G2300/202C10G2300/70C10G2400/04
Inventor 崔哲吴子明王仲义孙士可彭冲曹正凯范思强
Owner CHINA PETROLEUM & CHEM CORP
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