Poly(ester)carbonate and method for producing poly(ester)carbonate
A technology of polyester carbonate and manufacturing method, applied in the field of polycarbonate and polycarbonate manufacturing, capable of solving problems such as poor processability
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Embodiment 1
[0245] As the diol, 44.93 parts by mass of 2,2'-bis(2-hydroxyethoxy)-1,1'-binaphthyl (hereinafter abbreviated as BHEB) and 9,9-bis[4-(2-hydroxyl) were used. 43.85 parts by mass of ethoxy)phenyl]fluorene (hereinafter abbreviated as BPEF in some cases),
[0246] As an ester-forming derivative, 72.43 parts by mass of 2,2'-bis(carboxymethoxy)-1,1'-binaphthyl (hereinafter abbreviated as BCMB) was used,
[0247] As carbonate, 9.43 parts by mass of diphenyl carbonate (hereinafter sometimes abbreviated as DPC) was used,
[0248] After putting into a reactor equipped with a stirrer and a distillation apparatus, and performing nitrogen replacement three times, the jacket was heated to 200° C. to melt the raw materials. After complete dissolution, the pressure was reduced to 40 kPa over 20 minutes. Then, the temperature of the jacket was raised to 240°C at a rate of 60°C / hr. Thereafter, the pressure was reduced to 26 kPa over 20 minutes with the jacket kept at 240°C. Thereby, the est...
Embodiment 2
[0253] P compound 1 was changed to diethyl p-methylbenzylphosphonate (hereinafter sometimes abbreviated as P compound 2), and the ratio was 58.1×10 -3 Particles of polyester carbonate were obtained by the same method as in Example 1, except for the parts by mass. The physical properties of the obtained resin are shown in Table 1.
Embodiment 3
[0255] P compound 1 was changed to diethyl benzyl phosphonate (hereinafter sometimes abbreviated as P compound 3), and made 54.8×10 -3 Particles of polyester carbonate were obtained by the same method as in Example 1, except for the parts by mass. The physical properties of the obtained resin are shown in Table 1.
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