Nickel carbide/carbon nitride nanosheet photocatalytic material, preparation method and application thereof

A photocatalytic material, carbon nitride technology, applied in chemical instruments and methods, physical/chemical process catalysts, chemical/physical processes, etc., can solve the problems of high cost, insufficient absorption performance, poor conductivity, etc.

Inactive Publication Date: 2020-10-20
泰州市海创新能源研究院有限公司
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  • Abstract
  • Description
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Problems solved by technology

However, since g-C 3 N 4 The shortcomings of high charge carrier recombination rate, low quantum efficiency, small specific surface area, poor conductivity, and insufficient absorption performance above 460 nm make g-C 3 N 4 There are still obstacles in practical application
To improve g-C 3 N 4 For photocatalytic efficiency, metals such as platinum are often used as co-catalysts to improve the photocatalytic effect. However, platinum is a noble metal, and its high cost limits its application. Noble metal co-catalysts are promising and meaningful

Method used

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  • Nickel carbide/carbon nitride nanosheet photocatalytic material, preparation method and application thereof
  • Nickel carbide/carbon nitride nanosheet photocatalytic material, preparation method and application thereof
  • Nickel carbide/carbon nitride nanosheet photocatalytic material, preparation method and application thereof

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Embodiment

[0023] Example: including Ni 3 C / 2D g-C 3 N 4 Nano-heterojunction, the mass ratio of nickel carbide / carbon nitride is 5:100~25:100; the nickel carbide is a nano-particle, and the carbon nitride is a two-dimensional nano-sheet. Wherein, the mass ratio of nickel carbide / carbon nitride is 15:100.

[0024] The preparation of nickel carbide / carbon nitride nanosheet photocatalytic material comprises the following steps:

[0025] S1. Put melamine in a ceramic crucible with a cover, heat up to 550°C in a muffle furnace at a rate of 2°C / min and calcinate for 250min to obtain a yellow substance, grind the yellow substance into powder, and spread 400mg of the yellow powder on the In the uncovered ark, put it into a muffle furnace and heat up to 550°C at a rate of 10°C / min for calcination for 90 minutes to obtain a white powder material that is a two-dimensional carbon nitride nanosheet.

[0026] S2. Put 300 mg of nickel (II) acetate and 10 mL of oleylamine into a three-neck round bot...

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Abstract

The invention relates to a photocatalytic material, particularly to a metallic nickel carbide/carbon nitride nanosheet photocatalytic material, a preparation method and application thereof, and belongs to the technical field of nano materials and hydrogen production by water photolysis. In a nitrogen atmosphere, nickel acetylacetonate is subjected to low-temperature pyrolysis in olefinic amine toprepare high-quality Ni3C nanoparticles, and on the basis, a novel Ni3C/2D g-C3N4 nano heterojunction is successfully synthesized by adopting a simple two-step method, wherein the hydrogen productionperformance is obviously improved compared with the hydrogen production activity of single two-dimensional carbon nitride.

Description

technical field [0001] The invention relates to a photocatalytic material, in particular to a nickel carbide / carbon nitride nanosheet photocatalytic material, a preparation method and an application thereof, and belongs to the technical field of nanomaterials and hydrogen production by photolysis of water. Background technique [0002] With the advancement of science and technology and the advancement of industrialization, the quality of people's living standards has been significantly improved, but the ensuing energy crisis and environmental pollution have become thorny problems faced by today's social development. Therefore, how to solve the above problems reasonably and efficiently has become the focus of attention of researchers in environmental governance and energy development all over the world. Hydrogen energy is regarded as the clean energy with the most development potential in the 21st century. Human beings have been interested in the application of hydrogen energ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J27/24C01B3/04
CPCB01J35/004B01J27/24C01B3/042C01B2203/0277C01B2203/1058Y02E60/36
Inventor 陈瀚翔于亚辉许晖
Owner 泰州市海创新能源研究院有限公司
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