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A method for resourceful treatment of waste water produced by Bic

A technology for producing wastewater and a treatment method, applied in the field of wastewater treatment, can solve problems such as uncontrollable synthesis and poor product quality, and achieve the effects of good universality, improved performance, and superior thermal insulation performance.

Active Publication Date: 2021-10-26
NANJING UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the quality of chemicals is closely related to their raw materials. Therefore, the traditional method utilizes the by-products of Bic to synthesize various chemicals, which has problems such as poor product quality and uncontrollable synthesis.

Method used

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  • A method for resourceful treatment of waste water produced by Bic
  • A method for resourceful treatment of waste water produced by Bic
  • A method for resourceful treatment of waste water produced by Bic

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] A 呔k produces wastewater resource processing method, including the following steps:

[0046] S1: Tempened the useful amount of wastewater containing the by-product of the 呔k production process to 50 ° C, distilled under -0.09 MPa, concentrated to the thick liquid viscosity of 800 MPa.s at 25 ° C, and cool down to 30 ° C ;

[0047] S2: Centrifugation of the thick liquid obtained in the S1 step, remove salt substances such as NaCl to obtain a pale yellow viscous polymer, spare, such as figure 1 The description, but is not limited to, various structural forms of Figure;

[0048] S3: Add 30g pale yellow viscous polymer, 60 g of polyether polyol 4100, 10 g of polyether polyols, 0.5 g of dietholamine, 0.02 g of triethylamine, 0.02 g of triamiacin, 0.05 g of acetate Potassium, 2G water, mix evenly gave component a;

[0049] S4: Add a certain amount of curing agent PM200 to the component a: The addition of the curing agent is 1: 1, immediately mechanically stirred 240s, stir evenly, ...

Embodiment 2

[0051] A 呔k produces wastewater resource processing method, including the following steps:

[0052] S1: The wastewater containing a by-product produced by the chick production process was heated to 50 ° C, distilled under -0.09 mPa, concentrated to a thick liquid viscosity at 25 ° C for 800 MPa.s, and cooled to 30 ° C;

[0053] S2: Centrifugation of the thick liquid obtained in the S1 step to remove salt substances such as NaCl to obtain a pale yellow viscous polymer, spare;

[0054] S3: 20g pale yellow viscous polymer, 70 g of polyether polyol 450, 10 g of polyether polyol PPG-2000, 0.5 g of polyether polyol PPG-2000, 0.5 g of polyether polyol, 0.02 g of ethylene glycol, 0.02 g of othiol , 1.5 g of triamia diamine, 2G water, mix evenly gave component a;

[0055] S4: Add a certain amount of curing agent to the component A, component A: The addition mass ratio of the curing agent is 1: 1, immediately mechanically stirred 240 s, stir uniform, immediately pour the mold to start foam,...

Embodiment 3

[0057] A 呔k produces wastewater resource processing method, including the following steps:

[0058] S1: The wastewater containing the by-product produced by the chick production process was heated to 50 ° C, distilled under -0.09 MPa, concentrated to a thick liquid viscosity at 25 ° C for 500 MPa.s, and cooled to 30 ° C;

[0059] S2: Centrifugation of the thick liquid obtained in the S1 step to remove salt substances such as NaCl to obtain a pale yellow viscous polymer, spare;

[0060] S3: Add 30g pale yellow viscous polymer, 60 g of polyether polyol 450, 10 g of polyether polyol 4110, 10.5 g of polyether polyol 4110, 10.5 g of ethylene glycol, 0.02 g of octoctate, 1.5 G trioxide diamine, 2G water, mix evenly gave component a;

[0061] S4: Add a certain amount of curing agent to the component a, component A: The addition of the curing agent is 1: 0.2, immediately mechanically stirred 180s, stir uniform, immediately poured into the mold to start foam, and finally obtained polyureth...

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Abstract

The invention discloses a method for resourceful treatment of waste water from the production of Bic, comprising the following steps: S1: raising the temperature of the waste water containing by-products generated in the production process of Bick to 50°C, distilling under reduced pressure at -0.09MPa, and concentrating until the viscosity of the thick liquid is 500-1000mPa.s at 25°C, and cool down to 30°C; S2: Centrifuge the thick liquid obtained in step S1 to remove salts such as NaCl, and obtain a light yellow viscous polymer material, standby; S3: add light yellow viscous polymer, polyether polyol, crosslinking agent, surfactant, chain extender, catalyst, water in sequence according to the proportion, and mix evenly to obtain component A; S4: add Add a certain amount of curing agent to component A, stir it mechanically immediately, and pour it into the mold immediately after stirring evenly to start foaming, and finally obtain rigid polyurethane foam. The invention can effectively treat the waste water produced by Bick, and can also use its by-products to produce high-quality rigid polyurethane foam, thereby realizing turning waste into wealth and having good application prospects.

Description

Technical field [0001] The present invention relates to the field of sewage treatment, and in particular, to a method of producing wastewater resource treatment in a buckle. Background technique [0002] 呔 呔 is widely used in various types of synthetic materials, adhesives, modified epoxy resins, high-performance electrical insulating materials, electrical components, and PES coatings as well-known materials, adhesives, modified epoxy resins, high-performance electrical insulating materials, electrical components, and PES coatings, high-performance electrical insulating materials, electrical components, and PES coatings as their auxiliary, adhesive, modified epoxy resin, high-performance electrical insulating materials, electrical components, and PES coatings middle. At present, the 呔克 is mainly based on cyanic acid, epoxy chloropropane, and schubinic base, a ring-ring reaction under catalyst, and adding a spermate in the reaction, and performs a closed-loop reaction in the react...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08G18/66C08G18/48C08G18/64C08G18/32C08G101/00
CPCC08G18/3206C08G18/3275C08G18/4081C08G18/48C08G18/6415C08G18/6688C08G2101/00
Inventor 吕路吕飞王林平黄前霖张炜铭潘丙才
Owner NANJING UNIV
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