High-length-diameter-ratio tricalcium phosphate artificial bone meal bone repair material and preparation method thereof
A tricalcium phosphate, high aspect ratio technology, applied in chemical instruments and methods, phosphorus compounds, inorganic chemistry, etc., to achieve the effects of high yield, mild reaction conditions, and broad clinical application prospects
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Embodiment 1
[0036] A tricalcium phosphate artificial bone repair material with a high aspect ratio, the artificial bone powder bone repair material is rod-shaped tricalcium phosphate particles, and the surface has a porous structure with interconnected pores; the diameter of the artificial bone powder bone repair material is 35-40nm , with a length of 50-75 μm and an aspect ratio of 1.25×10 3 ~2.14×10 3 .
[0037] The preparation method of the above-mentioned high aspect ratio tricalcium phosphate artificial bone powder bone repair material comprises the following steps:
[0038] S1. First, configure the concentration of 0.3mol / L (NH 4 ) 2 HPO 4 solution and a concentration of 0.2mol / L Ca(NO 3 ) 2 solution;
[0039] Under stirring conditions, 30mL (NH 4 ) 2 HPO 4 The solution was added dropwise to 30ml Ca(NO 3) 2 In the solution, control the feeding time to complete within 30 minutes, and after stirring evenly, configure a mixed solution of calcium salt and phosphate with a Ca...
Embodiment 2
[0048] A high aspect ratio tricalcium phosphate artificial bone repair material, the artificial bone powder bone repair material is rod-shaped tricalcium phosphate particles, and the surface is a porous structure with interconnected pores; the diameter of the artificial bone powder bone repair material is 25-30nm , with a length of 85-95 μm and an aspect ratio of 2.83×10 3 ~3.80×10 3 .
[0049] The preparation method of the above-mentioned high aspect ratio tricalcium phosphate artificial bone powder bone repair material comprises the following steps:
[0050] S1. First, configure NaH with a concentration of 0.3mol / L 2 PO 4 solution and a concentration of 0.2mol / L Ca(NO 3 ) 2 solution;
[0051] Under stirring conditions, 20mL NaH 2 PO 4 The solution was added dropwise to 20ml Ca(NO 3 ) 2 In the solution, control the feeding time to complete within 40 minutes, and after stirring evenly, configure it into a mixed solution of calcium salt and phosphate with a Ca / P molar...
Embodiment 3
[0060] A tricalcium phosphate artificial bone repair material with a high aspect ratio, the artificial bone powder bone repair material is rod-shaped tricalcium phosphate particles, and the surface has a porous structure with interconnected pores; the artificial bone powder bone repair material has a diameter of 30-35nm , with a length of 60-80 μm and an aspect ratio of 1.71×10 3 ~2.67×10 3 .
[0061] The preparation method of the above-mentioned high aspect ratio tricalcium phosphate artificial bone powder bone repair material comprises the following steps:
[0062] S1. First, configure K with a concentration of 0.3mol / L 2 HPO 4 Solution and CaCl with a concentration of 0.2mol / L 2 solution;
[0063] Under stirring conditions, 20mL K 2 HPO 4 The solution was added dropwise to 20ml CaCl at a certain speed 2 In the solution, control the feeding time to complete within 20 minutes, and after stirring evenly, configure a mixed solution of calcium salt and phosphate with a C...
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