Water-soluble garlic oil for aquaculture as well as preparation method and application thereof
An aquaculture, garlic oil technology, applied in the directions of application, medical preparations with inactive ingredients, medical preparations containing active ingredients, etc. The effect of enhancing disease resistance immunity, simple preparation method, antibacterial and anti-inflammatory culture body
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[0035] In order to better understand the water-soluble garlic oil in the present invention, the present invention also provides a method for preparing aquaculture water-soluble garlic oil, and the preparation method comprises the following steps:
[0036] S1, the styrene-based phenol polyoxyethylene ether is added to the reactor in the reaction ratio according to the raw material ratio, and the emulsifies are stirred at a certain temperature to obtain a mixed emulsion;
[0037] S2, in accordance with the raw material ratio, add garlic oil to a solvent, stir, and obtain dispersion;
[0038] S3, adding the dispersion liquid obtained in step S2 and the mixed emulsion obtained in step S1 to a high-speed shear, and after stirring for a period of time, water soluble garlic oil is prepared.
[0039]In a particular embodiment of the invention, the temperature in step S1 is 20 to 40 ° C (such as 20 ° C, 22 ° C, 25 ° C, 28 ° C, 30 ° C, 32 ° C, 35 ° C, 38 ° C, 40 ° C); The stirred rate is fr...
Example Embodiment
[0043] Example 1
[0044] This example provides aquaculture water-soluble garlic oil, according to mass parts, water-soluble garlic oil including the following raw material ratio: 3 parts of styrene-phenol polyoxyethylene ether, sodium dodecyl benzene sulfonate 3 65 parts of xylene, 25 parts of garlic oil.
[0045] Among them, garlic oil includes a component of mass: propyl disulfide propylene 50%, sulfur sulfide depropylene, 17.2% triulfide sulfide, 2% vulcanized dipropylene, methyl vs. 0.8%.
[0046] This embodiment also provides a method for preparing aquaculture water-soluble garlic oil, including the following steps:
[0047] S1, adding styrene-phenol polyoxyethylene ether 30g to the reactor with sodium dodecyl benzene sulfonate, at 30 ° C, and mixed emulsion at 30 ° C, 800 r / min at 30 ° C.
[0048] S2, in accordance with the raw material ratio to add 650 g of xylene in xylene, 800 r / min for 0.3 h, resulting in dispersion;
[0049] S3, adding the dispersion obtained in st...
Example Embodiment
[0052] Example 2
[0053] This example provides aquaculture water-soluble garlic oil, according to mass parts, water-soluble garlic oil including the following raw material ratio: 3 parts of styrene-phenol polyoxyethylene ether, sodium dodecyl benzene sulfonate 3 60 parts of xylene, 5 pieces of No. 180, 25 parts of garlic oil.
[0054] Among them, garlic oil includes a component of mass: propyl disulfide 5%, 38.5% di-sulfide sulfide, 15%, sulfide sulfide 1%, methyl vs. 0.5%.
[0055] This embodiment also provides a method for preparing aquaculture water-soluble garlic oil, including the following steps:
[0056] S1, adding styrene-phenol polyoxyethylene ether 30g to the reactor with sodium dodecyl benzene sulfonate, at 30 ° C, and mixed emulsion at 30 ° C, 800 r / min at 30 ° C.
[0057] S2, in the mixed solvent of 600 g of xylene and 50 g of 180 solvent according to the raw material ratio, 800 r / min is stirred for 0.3 h, resulting in dispersion;
[0058] S3, adding the dispersi...
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