Positive electrode active material and lithium secondary battery comprising same
A positive electrode active material and secondary particle technology, applied in secondary batteries, active material electrodes, positive electrodes, etc., can solve problems such as poor high temperature stability, battery rupture, and fire
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Embodiment 1
[0143] In the NiCoAl(OH) prepared by co-precipitation reaction 2 (d(50) = 3.0 μm) and Li as a lithium compound 2 CO 3 After weighing and mixing with LiOH (Li / M ratio=1.05±0.05), the first heat treatment was carried out at 800°C for 12 hours, thereby preparing the 1.0 Ni 0.9 co 0.078 Al 0.022 o 2 composed of lithium-based composite oxides.
[0144] The lithium-based composite oxide prepared above was added to distilled water, and washed with water while maintaining the temperature. After the dehydration process, drying was performed at 150° C. in a vacuum atmosphere. Next, the dried lithium-based composite oxide was subjected to a second heat treatment at 700° C. for 12 hours to obtain a positive electrode active material.
Embodiment 2
[0146] The cathode active material was prepared in the same manner as in Example 1 except that the first heat treatment temperature was 850° C. in Example 1.
Embodiment 3
[0148] The cathode active material was prepared in the same manner as in Example 1 except that the first heat treatment temperature was 900° C. in Example 1.
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Abstract
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