Preparation method of reinforced Pebax mixed matrix membrane
A technology of mixed matrix membrane and casting solution, applied in the field of membrane separation, can solve the problem that the ideal selectivity is not very high
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Embodiment 1
[0041] In a closed autoclave, blow nitrogen; add 10g diallylamine hydrochloride, 6g 3-amino-4-mercaptoquinoline (CAS: 109543-48-8), 100g ethanol, add 3g sodium methoxide , heated and stirred to 55°C, reacted for 2 hours, evaporated to remove ethanol, and obtained synergist 1.
preparation Embodiment 2
[0043] In a closed autoclave, blow nitrogen; add 14g diallylamine hydrochloride, 8g 3-amino-4-mercaptoquinoline (CAS: 109543-48-8), 120g ethanol, add 5g sodium methoxide , heated and stirred to 62°C, reacted for 4 hours, evaporated to remove ethanol, and obtained synergist 2.
Embodiment 3
[0045] In a closed autoclave, blow nitrogen; add 17g diallylamine hydrochloride, 10g 3-amino-4-mercaptoquinoline (CAS: 109543-48-8), 130g ethanol, add 6g sodium methoxide , heated and stirred to 68°C, reacted for 5 hours, evaporated to remove ethanol, and obtained synergist 3.
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