MULTIPLEX ASSAY FOR DETERMINING beta-AMYLOID 42/40 RATIO IN HUMAN PLASMA SPECIMENS
An amyloid, ratio technology, applied in the preparation of test samples, measurement devices, biological tests, etc., can solve the problems of early AD detection and the uselessness of intervention
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[0147] Patient plasma samples were manually diluted in dilution buffer to dissociate Aβ42 and Aβ40 from endogenous plasma proteins. Thaw each patient sample first, then vortex well. To achieve a 1:10 dilution, 30 μl of each patient sample was pipetted into a 1.5 ml snap-top tube containing 270 μl of Quanterix 4-Plex Diluent (Quanterix Corp., Mass. Lexington, State). The diluted patient samples were allowed to equilibrate at room temperature for at least 30 minutes but no more than 4 hours prior to further processing.
[0148] Amyloid β peptide controls consist of Aβ42 (e.g., β-amyloid (Aβ) [1-42] (human), Invitrogen #03-112) and Aβ40 (e.g., amyloid β protein 1-40, Sigma Aldrich #A1075 -1MG) stock solution preparation. From these stock solutions, "analogues" and high, medium, low concentration control. Each control solution was diluted 1:10 (60 μl pipetted into 540 μl of dilution buffer solution (eg, Quanterix 4-Plex diluent)).
[0149] A series of calibrators were prepar...
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