Cannabis infused products with enhanced cannabinoid spectrum user experience
A cannabinoid, hemp-based technology in the field of cannabinoid-infused products with an enhanced cannabinoid profile user experience that addresses higher than expected consumption and lack of consistency
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[0243] The following examples describe some exemplary modes of making and practicing certain compositions described herein. It should be understood that these examples are for illustrative purposes only and are not intended to limit the scope of the compositions and methods described herein.
example 1
[0245] In this example, compositions containing emulsions with particle sizes >1000 nm (Formulation 1), 200 nm (Formulation 2) and 40 nm (Formulation 3) were prepared.
[0246] Cannabinoid-based emulsions with particle sizes of 40 nm and 200 nm are provided in Tables 1 and 2 below. Based on the formulations listed in Tables 1 and 2, cannabinoid-based emulsions with particle sizes >1000 nm were prepared without an additional sonication step. These exemplary formulations span the range from nanoemulsions to macroemulsions. The aforementioned emulsion was prepared as follows:
[0247] 1. Dissolve the water phase and oil phase ingredients separately using heat and agitation. In particular, the aqueous phase consists of water, Tween TM 80. Ascorbic acid and EDTA were formulated and mixed at 60°C for 30 minutes with a magnetic stir bar. Oil phase by Labrafac TM lipophile WL1349, Tocobiol TM , lecithin and THC distillate and mixed at 60°C for 30 minutes with a magnetic stir b...
example 2
[0258] In this example, a THC-containing composition was prepared with a particle size < 100 nm.
[0259] In a container, 1,000 mg of THC-containing cannabis oil was mixed with 50 mg of poly(ethylene glycol) monooleate and an appropriate amount of ethanol to obtain an oil phase mixture. The oil phase mixture was heated at 50°C until a liquid oil phase was obtained. In a separate container, dissolve 50 mg of sodium oleate in 20 mL of deionized water to form an aqueous phase mixture. The oil phase mixture was added to the water phase mixture and the combined mixture was mixed with a high shear mixer to obtain a coarse emulsion. Here T25 (IKA company, Stauffen, Germany) at 8,000 rpm for 5 minutes can be used. The coarse emulsion was mixed with a microfluidizer to further homogenize the emulsion and obtain a first THC-containing microencapsulated composition with a particle size of <100 nm. A Nano DeBEE (Westwood Corporation, MA, USA) at 20,000 psi for 8-12 cycles can be used h...
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