Melaleuca bracteata sachet and preparation method thereof
A technology of golden willow incense and golden willow incense, applied in the field of golden willow sachet and preparation thereof, can solve the problems that the sachet has no immune function, cannot improve the immunity of the body, etc., so as to improve the anti-oxidation function and improve the compatibility. , the effect of inhibiting agglomeration
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[0034] The invention provides a preparation method of golden willow sachet, comprising the following steps:
[0035] S1. Preparation of the golden willow extract: freeze-dry the golden willow leaves for 8-12 hours at a temperature of -10 to -20°C, then pulverize and pass through a 40-60 mesh sieve. An ethanol solution with a mass of 25-35 times, the volume fraction of ethanol in the ethanol solution is 50vol%-60vol%; then placed in a flash extractor and extracted at a voltage of 120-160V for 90-180s, and the obtained extract is subjected to suction filtration , then the filtrate obtained by suction filtration is subjected to precipitation treatment with an ethanol solution whose volume fraction of ethanol is 80vol%-95vol%, and the supernatant liquid obtained from the precipitation treatment is the S. chinensis extract;
[0036] S2. Fragrance masterbatch preparation: add the extract obtained in step S1 to the β-cyclodextrin aqueous solution heated to 50-60° C. with a concentrat...
Embodiment 1
[0042]A kind of golden willow sachet is prepared according to the following steps by adopting the following raw materials:
[0043] S1. Preparation of the golden willow extract: freeze-dry the golden willow leaves at -10°C for 12 hours, then pulverize and pass through a 40-mesh sieve, and add 25 times its mass of ethanol solution to the sieved golden willow leaves, In the ethanol solution, the volume fraction of ethanol is 60vol%; then it is placed in a flash extractor for extraction at 120V for 180s, the obtained extract is subjected to suction filtration, and then the filtrate obtained by suction filtration is 95vol% ethanol. The ethanol solution is subjected to precipitation treatment, and the supernatant liquid obtained from the precipitation treatment is the Salix chinensis extract;
[0044] S2. Fragrance master batch preparation: add the extract obtained in step S1 to the β-cyclodextrin aqueous solution with a concentration of 5wt% heated to 50°C, filter after stirring, ...
Embodiment 2
[0048] A kind of golden willow sachet is prepared according to the following steps by adopting the following raw materials:
[0049] S1. Preparation of S. japonica extract: freeze-dried S. japonica leaves at -20°C for 8 hours, then pulverized and sieved through a 60-mesh sieve, and 35 times the mass of ethanol solution was added to the sifted S. S. japonicus leaves, In the ethanol solution, the volume fraction of ethanol is 50vol%; then it is placed in a flash extractor for extraction at a voltage of 160V for 90s, the obtained extract is subjected to suction filtration, and then the filtrate obtained by suction filtration is filtered with a volume fraction of 80vol% ethanol. The ethanol solution is subjected to precipitation treatment, and the supernatant liquid obtained from the precipitation treatment is the Salix chinensis extract;
[0050] S2. Fragrance master batch preparation: add the extract obtained in step S1 to the β-cyclodextrin aqueous solution with a concentration...
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