Method for fabricating improved composite active black dyestuff

A manufacturing method and reactive black technology, applied in the field of dyes, can solve the problems of unfavorable environmental protection, insufficient lifting force, large amount of sewage, etc., and achieve the effect of reducing water consumption in production and application, improving solubility, and reducing the generation of sewage

Inactive Publication Date: 2005-12-28
无锡润新染料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The traditional reactive black dye is to mix the synthetic active navy blue and active orange after salting out and drying. The defects of this process are: 1. It takes up a lot of equipment; 2. Solid-liquid separation will generate a lot of sewage, which is not conducive to environmental protection; 3. The yield of mixed products is low, the solubility is only 80-100 g / L, the lifting force is not enough when applied, the level dyeing property is not good, it cannot dye dark colors, and it is easy to dye flowers

Method used

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  • Method for fabricating improved composite active black dyestuff
  • Method for fabricating improved composite active black dyestuff
  • Method for fabricating improved composite active black dyestuff

Examples

Experimental program
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Effect test

Embodiment 1

[0020] Embodiment 1, the improved compound reactive black dye manufacture method, after mixing 75 parts of reactive navy blue solution and 25 parts of reactive orange solution of synthesis, spray drying to obtain finished product.

Embodiment 2

[0021] Embodiment 2, the improved composite reactive black dye manufacturing method, after mixing 65 parts of reactive navy blue solutions, 30 parts of reactive orange solutions, and 5 parts of reactive red solutions and stirring evenly, spray drying to obtain finished products, wherein when synthesizing reactive navy blue, raw materials The proportioning ratio of H acid and p-(β-sulfate ethyl sulfone) aniline is controlled to be 0.35:1.

Embodiment 3

[0022] Embodiment 3, the improved compound reactive black dyestuff manufacturing method, after 80 parts of reactive navy blue solutions of synthesis, 18 parts of reactive orange solutions and 2 parts of reactive red solutions after nano-membrane treatment are mixed and stirred, spray-dried to obtain finished product, wherein When synthesizing active navy blue, the feed ratio of raw material H acid and p-(β-sulfate ethyl sulfone) aniline is controlled to 0.4:1, and nano-membrane concentration is carried out.

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Abstract

The improved compound reactive black dye manufacturing method relates to the field of dyes. The synthetic reactive navy blue solution and reactive orange solution are mixed and evenly sprayed and dried. In this wet blending process, the reactive orange dye does not need to be salted out and is directly blended with the solution without Salt-out sewage is produced, and the solubility is greatly improved; the hue is similar to the reactive black KN-G2RC, which solves the shortcomings of KN-G2RC that cannot dye dark colors and the lifting power is not high; the solubility of the product reactive black reaches 180-200 g / L, and the lifting power High, good blackness, good level dyeing, dyeing cloth is not flowery, can dye dark colors, light fastness reaches 4 grades, soaping fastness 4-5 grades, rubbing fastness 4 grades, ironing fastness 4- Level 5.

Description

technical field [0001] The invention relates to the field of dyes, and refers to a new method for manufacturing composite reactive black dyes. technical background [0002] The traditional reactive black dye is to mix the synthetic reactive navy blue and reactive orange after salting out and drying. The defects of this process are: 1. It takes up a lot of equipment; 2. Solid-liquid separation will generate a lot of sewage, which is not conducive to environmental protection; 3. The yield of mixed products is low, the solubility is only 80-100 g / L, the lifting power is not enough when applied, the level dyeing property is not good, it cannot dye dark colors, and it is easy to dye flowers. Contents of the invention [0003] The present invention just aims at overcoming above-mentioned deficiency, provides a kind of improved compound reactive black dyestuff manufacture method, the product produced by this method has bright color, high solubility, low directness, good compatibi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09B67/24
Inventor 史锦锋
Owner 无锡润新染料有限公司
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