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Bulk polymerization imploding reaction prevention device

A bulk polymerization and reaction device technology, applied to pressure vessels used in chemical processes, etc., can solve problems such as low output, difficult removal of reaction products, and unsatisfactory heat exchange efficiency

Inactive Publication Date: 2006-07-05
PIPECHINA SOUTH CHINA CO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the heat exchange efficiency of this kind of device is not ideal, the reaction product is difficult to take out, the output is low, and the production efficiency is not high

Method used

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  • Bulk polymerization imploding reaction prevention device
  • Bulk polymerization imploding reaction prevention device
  • Bulk polymerization imploding reaction prevention device

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Embodiment 1: its composition is as figure 1 . The drum 2 of the reaction device is made of stainless steel, with a diameter of 1m and a length of 2m. The rotating speed is controlled by a speed changer, and the rotational speed of the drum 2 is 0.5m / min. It consists of 2 sets of reactors. The feeder 1 is in the shape of a flat mouth funnel, and the length is 2m; the diameter of the support wheel 3 is 0.1m, and the length is 2m, a total of 6 pieces, and one piece is installed every 30° from the right end of the horizontal horizontal center line of the drum 2; the diameter of the guide wheel 5 is 0.2m , 2m long, installed at 15° below the left end of the horizontal horizontal centerline of the drum 2. The second set of reactors is located at the bottom left of the first set of reactors, and its horizontal vertical centerline is 0.7m away from the horizontal vertical centerline of the first set of reactors. 6 supporting rollers 3 are installed on the same position of w...

Embodiment 2

[0028] Embodiment 2: Consists of a set of reactors. The drum 2 is made of stainless steel, with a diameter of 2m and a length of 3m, and its rotational speed is 0.25m / min; the feeder 1 is in the shape of a funnel with a flat mouth, and the length is 3m; the supporting roller 3 has a diameter of 0.2m, a length of 3m, and 6 supporting rollers 3 Install evenly every 30° from the right end of the horizontal horizontal centerline of the drum 2; the guide wheel 5 has a diameter of 0.4m and a length of 3m, and is installed at 15° below the left end of the horizontal horizontal centerline of the drum 2.

[0029] In the present invention, polymer monomers and catalysts are mixed and evenly distributed on the drum 2 with a flowing heat exchange medium for heat dissipation to carry out polymerization reaction. The heat exchange is good, detonation can be completely prevented, continuous production is possible, and production efficiency is high. , The polymerization product can be automat...

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PUM

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Abstract

The invention provides a reaction device. It assembles a set of reactors below the filler in the container, or further it is connected with one or several reactors in series, under the lowest grade of reactor there has a transmission belt and finished product cabinet. The reactor is made up of rotation wheel, supporting wheel, scraper, guiding wheel and heat exchanging media inlet and outlet. The device has a high heat exchanging efficiency, and it is very simple.

Description

technical field [0001] The invention is a bulk polymerization anti-explosion polymerization reaction device used for preventing explosion polymerization in the bulk polymerization process. Involves the general field of chemical installations and piping systems. Background technique [0002] The bulk polymerization process is a process widely used in the synthesis of ultra-high molecular weight polymers. However, most polymerization reactions are exothermic reactions. If the heat generated by the reaction cannot be discharged in time, implosion polymerization will easily occur, which will affect the performance of the polymer. In order to prevent detonation, two methods are usually adopted. One is to use microcapsule technology, that is, to use special coating materials to make microcapsules (particle size less than 0.25cm) made of polymer monomers and catalysts into the heat exchange medium. It is a continuous phase and has a large volume, which can quickly remove the hea...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J3/04
Inventor 李国平张秀杰刘兵张金岭艾慕阳鲍旭晨
Owner PIPECHINA SOUTH CHINA CO