Photo sensitive composition and negative lithographic printing plate
A photosensitive composition and resin technology, applied in lithographic printing equipment, printing, printing technology, etc., can solve the problems of photosensitive layer film strength and storage stability, and achieve excellent printing resistance and storage stability, and high practicality Excellent performance and film strength
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Synthetic example 1
[0431] Synthesis Example 1: Compound P-1
[0432] In a flask, mix monomer A-1 (0.8 mol), methacrylic acid (0.2 mol), V-65 (manufactured by Wako Pure Chemical Industries, Ltd., an azo thermal polymerization initiator) (0.03 mol), N,N-di Methylacetamide (1 L), stirred at 70°C for 5 hours. After the reaction, the reaction solution was slowly added into 5 L of water while stirring, and a white powder was precipitated. The powder was filtered and dried to obtain P-1 in 90% yield. The structure of this substance was confirmed by NMR, IR, and GPC.
Synthetic example 2
[0433] Synthesis Example 2: Compound P-8
[0434] Mix A-81 (0.6 mol), acrylic acid (0.4 mol), V-65 (manufactured by Wako Pure Chemical Industries, Ltd., azo-based thermal polymerization initiator) (0.02 mol), and N,N-dimethylacetamide in a flask (1 L), stirred at 70°C for 5 hours. After the reaction, the reaction solution was slowly added into 5 L of water while stirring, and a white powder was precipitated. The powder was filtered and dried to afford P-9 in 85% yield. The structure of this substance was confirmed by NMR, IR, and GPC.
Synthetic example 3
[0435] Synthesis Example 3: Compound P-16
[0436] Mix A-17 (0.5 mol), methacrylic acid (0.3 mol), benzyl acrylate (0.2 mol), V-65 (manufactured by Wako Pure Chemical Industries, Ltd., azo thermal polymerization initiator) (0.03 mol) in a flask ), N,N-dimethylacetamide (1L), stirred at 70°C for 5 hours. After the reaction, the reaction solution was slowly added into 5 L of water while stirring, and a white powder was precipitated. The powder was filtered and dried to obtain P-16 in a yield of 90%. The structure of this substance was confirmed by NMR, IR, and GPC.
[0437] As described above, all the polymers shown in the specific examples can be synthesized.
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