Process for growing Ge nanoline by aluminium oxide template
An alumina template, germanium nanowire technology, applied in the direction of magnetic materials, electrical components, circuits, etc., can solve the problems of inability to array, large distribution range of diameter and length, inconsistent orientation, etc.
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[0010] Example Two-step anodic oxidation is used to prepare nanoporous alumina templates. During anodic oxidation, a lead plate is used for the cathode, and an aluminum sheet with a purity of 99.99% is used for the anode. First, the aluminum sheet is ultrasonically cleaned, annealed, alkaline degreasing, and acidic And the electrolytic polishing process to obtain a clean and smooth aluminum sheet, using a concentration of 0.3mol / L oxalic acid solution at room temperature with a constant DC voltage of 40V for the first anodic oxidation of aluminum, after 12 hours of oxidation, use 8%CrO 3 +6%H 3 PO 4 The solution was corroded at a temperature of 60°C for 10 hours to remove the oxide layer, and then the second step of anodic oxidation was performed under the same conditions as the first step to form a hole array of porous alumina, and finally HgCl 2 solution and H 3 PO 4 The solution removes...
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