The application relates to a doped
optical fiber preparation process and discloses a high-uniformity and high-concentration Pr 3+ The application discloses a preparation method of a doped
quartz-based glass
optical fiber.
Rare earth oxide Pr2O3, silica
powder SiO2 and aluminum
oxide Al2O3 are weighed, mechanically mixed, ball milled, dried, sieved, pre-sintered to be transformed into
cristobalite, drawn into a glass rod containing a core by using a tube melting method, and processed to remove the outer cladding of the glass rod to obtain a core rod with adjustable
diameter. The tube rod method is combined with a high-purity
quartz tube to form an
optical fiber preform rod. Finally, the optical
fiber preform rod has high uniformity, low loss and
high concentration of Pr 3+ The application discloses a drawing method of a doped
quartz optical
fiber. The aluminum
oxide Al2O3 is introduced to improve the
solubility of the
rare earth ion Pr 3+ in the quartz glass and reduce the
melting point of the quartz
raw material. The
rare earth doping concentration is adjustable. The
raw material is transformed into
cristobalite by pre-
sintering, and the effect of reducing the bubbles of the core glass and improving the uniformity of the core glass is remarkable by combining the
vacuum tube melting method.