Preparation method of water-base acid Co ferrite CoFe2O4 magnetic solution
An acid cobalt iron, magnetic liquid technology, applied in magnetic liquids, chemical instruments and methods, cobalt compounds, etc., can solve the problems of high concentration of harmful components in waste, complex preparation process, high cost, and achieve less waste and preparation. Simple method and low cost effect
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[0021] Example 1: (I) Dosing
[0022] Solution 1 uses FeCl 3 ·6H 2 O (purity 98.06%) with 1M concentration of FeCl 3 Aqueous solution.
[0023] Solution 2 uses Co(NO 3 ) 2 ·H 2 O (purity 97.00%) with 2M concentration of Co(NO 3 ) 2 Aqueous solution, and press [5M HCl / 1 liter Co(NO 3 ) 2 Aqueous solution] Add an appropriate amount of HCl in proportion.
[0024] Solution 3 Use NaOH (purity 96.00%) to prepare a 0.7M NaOH aqueous solution. (II) Mixed
[0025] Solution 1 and solution 2 are selected according to the ratio of Fe to Co molar ratio of 2:1, and solution 1 is poured into solution 2 to obtain solution 2'.
[0026] Solution 3 is selected according to the volume ratio of solution 2'to solution 3 of 1:11. Pour solution 2'into solution 3 quickly (not more than 10 seconds) with stirring. After stirring for 10 minutes, solution 3'is obtained. (III) Reaction
[0027] Under stirring conditions, the solution 3'was heated to boiling and kept boiling for 1 minute. Then stop heating and ...
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