Aluminum hydroxide, aluminum hydroxide slurry and resin composition containing the same, and method for producing the same
A technique for producing aluminum hydroxide and its manufacturing method, which is applied in the fields of alumina/hydroxide preparation, alumina/aluminum hydroxide, chemical instruments and methods, etc., which can solve the problems that it is difficult to obtain sufficient surface hardness and achieve improved The effect of surface hardness
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example 1
[0051] [Preparation of Alumina Intermediate]
[0052] Alumina ("C-31" product manufactured by Sumitomo Chemical Company, whose main crystal phase is gibbsite) is ground with a vibrating grinder, and then quickly calcined in the air at 700 degrees Celsius to form oxidation Aluminum intermediate, its main crystal phase is ρ, average particle diameter is 3 microns, the electron micrograph is as figure 1 Shown.
[0053] [Preparation of Aluminum Hydroxide]
[0054] Mix 56 grams of the above alumina intermediate with 744 grams of water, then add 161.6 grams of magnesium acetate tetrahydrate (reagent grade, manufactured by Wako Pure Chemical Co., Ltd.) and dissolve it to form an aqueous magnesium acetate solution A slurry of alumina intermediates is dispersed in it. The concentration of magnesium acetate in the aqueous solution was 0.94 mol / liter.
[0055] The slurry was placed in a pressure cooker (manufactured by Taiatsu Glass Kogyo K.K.) with a capacity of 1 liter, and subjected to h...
example 2
[0063] The magnesium acetate in Example 1 was replaced by magnesium acetate tetrahydrate (the concentration of magnesium acetate in the aqueous solution was 0.93 mol / L), and the other conditions were the same as in Example 1 to prepare aluminum hydroxide. The formed aluminum hydroxide contains 12wt% of magnesium, its main crystal phase is gibbsite, the main particle shape is needle-like, the average length is 150nm, the average width is 20nm, and the aspect ratio is 7.5. The average particle size of aluminum hydroxide is 3 microns, and the electron micrograph is as follows image 3 Shown. Using the aluminum hydroxide formed by this method, the same resin composition as in Example 1 can be obtained.
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