Process for the constrained sintering of a pseudo-symmetrically configured low temperature cofired ceramic structure
一种陶瓷、低温的技术,应用在陶瓷层状产品、化学仪器和方法、多层电路制造等方向,能够解决提高材料、设备和加工成本、底部导体不能共加工等问题
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Embodiment 1
Glass density 4.45g / cc
Alumina density 4.02g / cc
[0087] The content of the above filler and glass represents the solid formulation of the primary belt and the restraint belt. Use these materials
[0088] Experiment #1
Elementary#1 / Restriction#1 / Elementary#1 / Restriction#2 / Elementary#1
Layer ratio = 3 / 1 / 6 / 1 / 3
Restriction band thickness = 4.0 mils
Primary tape thickness = 4.5 mils
Total / Constrained Belt Thickness Ratio=7.8
Test #2
Elementary#1 / Restriction#1 / Elementary#1 / Restriction#2 / Elementary#1
Layer ratio = 2 / 1 / 4 / 1 / 2
The thickness of the restraint band = 4.0 mils
Primary tape thickness = 4.5 mils
Total / Constrained Belt Thickness Ratio=5.5
Trial #3
Elementary#1 / Restriction#1 / Elementary#1 / Restriction#2 / Elementary#1
Layer ratio=3 / 1 / 4 / 1 / 3
Restriction band thickness = 4.0 mils
Primary tape thickness = 4.5 mils
Total / Constrained Belt Thickness Ratio=6.6
Trial #4
...
Embodiment 2
[0093] The primary #2 tape (4.5 mils thick) was paired with two different restraint tape compositions (restraint #1 and restraint #2), which have the same total / restraint tape thickness ratio, as in Example 1 Shown.
[0094] Glass:
Filler: Al 2 O 3 (D50=2.8 microns)
Filler content 33.9% by volume
SiO 2
54.50
Weight%
Na 2 O
2.20
Al 2 O 3
12.72
Li 2 O
0.24
B 2 O 3
8.32
SrO
2.94
CaO
16.63
K 2 O
1.47
MgO
0.98
Glass density 2.55g / cc
Alumina density 4.02g / cc
Trial #5
Elementary#2 / Restriction#1 / Junior#2 / Restriction#2 / Junior#2
Layer ratio = 3 / 1 / 6 / 1 / 3
Restriction band thickness = 4.0 mils
Primary tape thickness = 4.5 mils
Total / Constrained Belt Thickness Ratio=7.8
Test #6
Elementary#2 / Restriction#1 / Junior#2 / Restriction#2 / Junior#2
Layer ratio = 2 / 1 / 4 / 2 / 1
The...
Embodiment 3
[0098] This embodiment uses restraint belts #2 and 3 and primary belt #2. Regarding the dielectric constant k value, the confinement band #2 is higher than the primary band #2, and the dielectric constant of the primary band #2 and the confinement band #3 are similar.
[0099] Glass:
[0100] In the belt furnace, after firing at 850°C, all samples are relatively flat, showing the following x, y shrinkage %: test #10 is 0.42%, test #11 is 0.22%, test #12 is 0.33%, test #13 is 0.09%. Comparing the above 13 experiments, it is obvious that the combination of primary belt #2 and restraint belts #1 and #2 provides the most effective x, y shrinkage control.
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